1-Phenyl-3-nitropropane

Base Information

• Chemical Name: 1-Phenyl-3-nitropropane
• CAS No.: 22818-69-5
• Molecular Formula: C9H11NO2
• Molecular Weight: 165.192
• Hs Code.: 2904209090
• Mol file: 22818-69-5.mol

Synonyms:3-phenylnitropropane;3-phenyl-1-nitropropane;

Chemical Property of 1-Phenyl-3-nitropropane

Chemical Property:

• PSA: 45.82000
• LogP: 2.41910

Purity/Quality:

95% ^*data from raw suppliers

1-Nitro-3-phenylpropane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Phenyl-3-nitropropane

There total 15 articles about 1-Phenyl-3-nitropropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

3-nitro-1-phenyl-propan-1-one (62847-52-3) → (3-nitropropyl)benzene (22818-69-5)

Guidance literature:

With triethylsilane; trifluoroacetic acid; at 20 ℃; Inert atmosphere;

Reference yield: 85.0%

3-Phenylpropan-1-amine (2038-57-5) → (3-nitropropyl)benzene (22818-69-5)

Guidance literature:

With silica gel; ozone; In neat (no solvent); at -60 ℃; for 0.25h;

DOI:10.1021/acs.joc.1c00768

Reference yield: 76.0%

1-Bromo-3-phenylpropane (637-59-2) → (3-nitropropyl)benzene (22818-69-5)

Guidance literature:

With silver nitrate; In diethyl ether; at 0 - 20 ℃; for 22h;

upstream raw materials:

1-iodo-3-phenylpropan

1-Bromo-3-phenylpropane

Nitroethane

benzyl bromide

Downstream raw materials:

1-nitro-2-(4-nitrobenzyl)ethane

1-[4-(3-nitro-propyl)-phenyl]-ethanone

3-phenyl-propionaldehyde

4-(3-Nitro-propyl)-benzenesulfonic acid