ethyl N-[(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methyl]carbamate

Base Information

Chemical Name:ethyl N-[(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methyl]carbamate
CAS No.:1227674-39-6
Molecular Formula:C₂₄H₂₉Br₂I₂NO₂
Molecular Weight:777.117
Hs Code.:

Synonyms:ethyl N-[(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methyl]carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl N-[(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methyl]carbamate

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Technology Process of ethyl N-[(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methyl]carbamate

There total 6 articles about ethyl N-[(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 1227674-38-5
(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tertbutylphenyl)chloromethane

: 51-79-6
urethane

: 1227674-39-6
ethyl N-[(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methyl]carbamate

Guidance literature:: With silver tetrafluoroborate; In 1,4-dioxane; at 60 - 100 ℃;
DOI:10.1002/poc.1651

Reference yield:

: 1227674-36-3
4-tert-butyl-2,6-diiodobenzaldehyde

: 1227674-39-6
ethyl N-[(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether; hexane / 5 h / -78 °C

1.2: -78 - 20 °C

2.1: thionyl chloride / 20 °C

3.1: silver tetrafluoroborate / 1,4-dioxane / 60 - 100 °C

With silver tetrafluoroborate; n-butyllithium; thionyl chloride; In 1,4-dioxane; diethyl ether; hexane;
DOI:10.1002/poc.1651

Reference yield:

: 1227674-34-1
4-tert-butyl-2,6-diiodobenzyl acetate

: 1227674-39-6
ethyl N-[(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methyl]carbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / methanol / 3 h / 20 °C

2.1: pyridinium chlorochromate / dichloromethane / 20 °C

3.1: n-butyllithium / diethyl ether; hexane / 5 h / -78 °C

3.2: -78 - 20 °C

4.1: thionyl chloride / 20 °C

5.1: silver tetrafluoroborate / 1,4-dioxane / 60 - 100 °C

With silver tetrafluoroborate; n-butyllithium; thionyl chloride; potassium carbonate; pyridinium chlorochromate; In 1,4-dioxane; methanol; diethyl ether; hexane; dichloromethane;
DOI:10.1002/poc.1651