1-O-methyl-3,5-di-O-benzyl-2-O-propionyl-β-D-ribofuranose-2,3,4,5,5'-2H5

Base Information

Chemical Name:1-O-methyl-3,5-di-O-benzyl-2-O-propionyl-β-D-ribofuranose-2,3,4,5,5'-2H5
CAS No.:372176-97-1
Molecular Formula:C₂₃H₂₈O₆
Molecular Weight:405.432
Hs Code.:

Synonyms:1-O-methyl-3,5-di-O-benzyl-2-O-propionyl-β-D-ribofuranose-2,3,4,5,5'-2H5

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Chemical Property of 1-O-methyl-3,5-di-O-benzyl-2-O-propionyl-β-D-ribofuranose-2,3,4,5,5'-2H5

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Technology Process of 1-O-methyl-3,5-di-O-benzyl-2-O-propionyl-β-D-ribofuranose-2,3,4,5,5'-2H5

There total 6 articles about 1-O-methyl-3,5-di-O-benzyl-2-O-propionyl-β-D-ribofuranose-2,3,4,5,5'-2H5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 38869-24-8
cesium propionate

: 372176-96-0
1-O-methyl-3,5-di-O-benzyl-2-O-trifluoromethanesulfonyl-β-D-arabinofuranose-2,3,4,5,5'-2H5

: 372176-97-1
1-O-methyl-3,5-di-O-benzyl-2-O-propionyl-β-D-ribofuranose-2,3,4,5,5'-2H5

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 36h;
DOI:10.1021/jo010097n

Reference yield:

: 372176-90-4
C₂₀H₁₉⁽²⁾H₅O₅

: 372176-97-1
1-O-methyl-3,5-di-O-benzyl-2-O-propionyl-β-D-ribofuranose-2,3,4,5,5'-2H5

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / pyridine

2: 91 percent / NaOMe / methanol / 0.5 h / 20 °C

3: 84 percent / DMAP; pyridine / CH₂Cl₂ / 3 h / 0 °C

4: 80 percent / dimethylformamide / 36 h / 20 °C

With pyridine; dmap; sodium methylate; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo010097n

Reference yield:

: 372176-95-9
1-O-methyl-3,5-di-O-benzyl-β-D-arabinofuranose-2,3,4,5,5'-2H5

: 372176-97-1
1-O-methyl-3,5-di-O-benzyl-2-O-propionyl-β-D-ribofuranose-2,3,4,5,5'-2H5

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / DMAP; pyridine / CH₂Cl₂ / 3 h / 0 °C

2: 80 percent / dimethylformamide / 36 h / 20 °C

With pyridine; dmap; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo010097n