platinum(II) 5-(4-methoxycarbonylbiphenyl)-10,15,20-triphenylporphyrin

Base Information

Chemical Name:platinum(II) 5-(4-methoxycarbonylbiphenyl)-10,15,20-triphenylporphyrin
CAS No.:1370414-13-3
Molecular Formula:C₅₂H₃₄N₄O₂Pt
Molecular Weight:941.948
Hs Code.:

Synonyms:platinum(II) 5-(4-methoxycarbonylbiphenyl)-10,15,20-triphenylporphyrin

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Chemical Property of platinum(II) 5-(4-methoxycarbonylbiphenyl)-10,15,20-triphenylporphyrin

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Technology Process of platinum(II) 5-(4-methoxycarbonylbiphenyl)-10,15,20-triphenylporphyrin

There total 1 articles about platinum(II) 5-(4-methoxycarbonylbiphenyl)-10,15,20-triphenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 5-(4-methoxycarbonylbiphenyl)-10,15,20-triphenylporphyrin

: 10025-65-7
platinum(II) chloride

: 1370414-13-3
platinum(II) 5-(4-methoxycarbonylbiphenyl)-10,15,20-triphenylporphyrin

Guidance literature:: In benzonitrile; porphyrin dissolved in PhCN; PtCl2 added; refluxed under Ar for 6-8 h; solvent evapd. in vac.; residue purified by column chromy. on silica gel(CH2Cl2 eluent);
DOI:10.1021/jp301345h

Reference yield: 96.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 1370414-13-3
platinum(II) 5-(4-methoxycarbonylbiphenyl)-10,15,20-triphenylporphyrin

: 1370414-14-4
platinum(II) 5-(4-carboxybiphenyl)-10,15,20-triphenylporphyrin

Guidance literature:: With KOH; In tetrahydrofuran; ethanol; to Pt complex in mixt. of THF/EtOH added pellet of KOH; stirred at room temp. for 8 h; solvent removed in vac., solid dissolved in water; soln. filtered; neutralized by HCl; ppt. collected by centrifugation; washed with water; dried in vac.;
DOI:10.1021/jp301345h