methyl 5-[5-(2,4-dimethoxy-benzylamino)-2,4-diisobutoxy-benzoylamino]-2,4-dimethoxybenzoate

Base Information

Chemical Name:methyl 5-[5-(2,4-dimethoxy-benzylamino)-2,4-diisobutoxy-benzoylamino]-2,4-dimethoxybenzoate
CAS No.:915184-69-9
Molecular Formula:C₃₄H₄₄N₂O₉
Molecular Weight:624.731
Hs Code.:

Synonyms:methyl 5-[5-(2,4-dimethoxy-benzylamino)-2,4-diisobutoxy-benzoylamino]-2,4-dimethoxybenzoate

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Chemical Property of methyl 5-[5-(2,4-dimethoxy-benzylamino)-2,4-diisobutoxy-benzoylamino]-2,4-dimethoxybenzoate

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Technology Process of methyl 5-[5-(2,4-dimethoxy-benzylamino)-2,4-diisobutoxy-benzoylamino]-2,4-dimethoxybenzoate

There total 6 articles about methyl 5-[5-(2,4-dimethoxy-benzylamino)-2,4-diisobutoxy-benzoylamino]-2,4-dimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874210-18-1
2,4-diisobutoxy-5-nitrobenzoic acid

: 915184-69-9
methyl 5-[5-(2,4-dimethoxy-benzylamino)-2,4-diisobutoxy-benzoylamino]-2,4-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: (COCl)2; DMF / CH₂Cl₂ / Heating

2.1: 2.96 g / Et₃N / CH₂Cl₂ / 20 Torr

3.1: H₂ / Pd/C / ethanol; CHCl₃

4.1: ethanol / 20 °C

4.2: 3.84 g / NaBH₄ / ethanol / 12 h

With oxalyl dichloride; hydrogen; triethylamine; N,N-dimethyl-formamide; palladium on activated charcoal; In ethanol; dichloromethane; chloroform;
DOI:10.1021/ol062103d

Reference yield:

: 2,4-diisobutoxy-5-nitro-benzoyl chloride

: 915184-69-9
methyl 5-[5-(2,4-dimethoxy-benzylamino)-2,4-diisobutoxy-benzoylamino]-2,4-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2.96 g / Et₃N / CH₂Cl₂ / 20 Torr

2.1: H₂ / Pd/C / ethanol; CHCl₃

3.1: ethanol / 20 °C

3.2: 3.84 g / NaBH₄ / ethanol / 12 h

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; chloroform;
DOI:10.1021/ol062103d

Reference yield:

: 915184-68-8
methyl 5-(2,4-diisobutoxy-5-nitrobenzoylamino)-2,4-dimethoxybenzoate

: 915184-69-9
methyl 5-[5-(2,4-dimethoxy-benzylamino)-2,4-diisobutoxy-benzoylamino]-2,4-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂ / Pd/C / ethanol; CHCl₃

2.1: ethanol / 20 °C

2.2: 3.84 g / NaBH₄ / ethanol / 12 h

With hydrogen; palladium on activated charcoal; In ethanol; chloroform;
DOI:10.1021/ol062103d