Nα-(2,6-dichlorobenzoyl)-4-{6-(N-formyl-N-methylamino-methyl)-quinazoline-2,4[1H,3H]-dion-3-yl}-L-phenylalanine isopropyl ester

Base Information

Chemical Name:Nα-(2,6-dichlorobenzoyl)-4-{6-(N-formyl-N-methylamino-methyl)-quinazoline-2,4[1H,3H]-dion-3-yl}-L-phenylalanine isopropyl ester
CAS No.:1029395-37-6
Molecular Formula:C₃₀H₂₈Cl₂N₄O₆
Molecular Weight:611.482
Hs Code.:

Synonyms:Nα-(2,6-dichlorobenzoyl)-4-{6-(N-formyl-N-methylamino-methyl)-quinazoline-2,4[1H,3H]-dion-3-yl}-L-phenylalanine isopropyl ester

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Chemical Property of Nα-(2,6-dichlorobenzoyl)-4-{6-(N-formyl-N-methylamino-methyl)-quinazoline-2,4[1H,3H]-dion-3-yl}-L-phenylalanine isopropyl ester

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Technology Process of Nα-(2,6-dichlorobenzoyl)-4-{6-(N-formyl-N-methylamino-methyl)-quinazoline-2,4[1H,3H]-dion-3-yl}-L-phenylalanine isopropyl ester

There total 2 articles about Nα-(2,6-dichlorobenzoyl)-4-{6-(N-formyl-N-methylamino-methyl)-quinazoline-2,4[1H,3H]-dion-3-yl}-L-phenylalanine isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 857870-47-4
4-amino-Nα-(2,6-dichlorobenzoyl)-L-phenylalanine isopropyl ester

: 1029395-41-2
2-amino-5-(N-formyl-N-methylamino-methyl) benzoic acid methyl ester

: 530-62-1
1,1'-carbonyldiimidazole

: 1029395-37-6
Nα-(2,6-dichlorobenzoyl)-4-{6-(N-formyl-N-methylamino-methyl)-quinazoline-2,4[1H,3H]-dion-3-yl}-L-phenylalanine isopropyl ester

Guidance literature:: 4-amino-Nα-(2,6-dichlorobenzoyl)-L-phenylalanine isopropyl ester; 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 5 - 10 ℃;

2-amino-5-(N-formyl-N-methylamino-methyl) benzoic acid methyl ester; In N,N-dimethyl-formamide; at 60 ℃; for 6h; Product distribution / selectivity;

Reference yield:

: 1029395-25-2
2-amino-5-[[formyl(methyl)amino]methyl]benzoic acid

: 1029395-77-4
4-carboxyl-Nα-(2,6-dichlorobenzoyl)-L-phenylalanine isopropyl ester

: 1029395-37-6
Nα-(2,6-dichlorobenzoyl)-4-{6-(N-formyl-N-methylamino-methyl)-quinazoline-2,4[1H,3H]-dion-3-yl}-L-phenylalanine isopropyl ester

Guidance literature:: 4-carboxyl-Nα-(2,6-dichlorobenzoyl)-L-phenylalanine isopropyl ester; With diphenylphosphoranyl azide; triethylamine; In acetonitrile; at 60 ℃; for 1h;

2-amino-5-[[formyl(methyl)amino]methyl]benzoic acid; In acetonitrile; at 90 ℃; for 12h;

With 1,1'-carbonyldiimidazole; In acetonitrile; for 1.5h; Product distribution / selectivity;