3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl)>-β-D-erythro-heptafuranuronic acid

Base Information

Chemical Name:3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl)>-β-D-erythro-heptafuranuronic acid
CAS No.:75863-44-4
Molecular Formula:C₂₁H₂₄N₂O₇
Molecular Weight:416.431
Hs Code.:

Synonyms:3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl)>-β-D-erythro-heptafuranuronic acid

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Chemical Property of 3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl)>-β-D-erythro-heptafuranuronic acid

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Technology Process of 3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl)>-β-D-erythro-heptafuranuronic acid

There total 6 articles about 3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl)>-β-D-erythro-heptafuranuronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 75863-42-2
benzyl 3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl>-β-D-erythro-hept-5-enofuranuronate

: 75863-44-4
3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl)>-β-D-erythro-heptafuranuronic acid

Guidance literature:: With hydrogen; platinum(IV) oxide; In acetic acid; for 3h; Ambient temperature;
DOI:10.1021/jo00316a021

Reference yield:

: 106-43-4
para-chlorotoluene

: 75863-44-4
3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl)>-β-D-erythro-heptafuranuronic acid

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1) 1h, cold, 2) 40h at ambient temp.

2: 93 percent / H₂ / PtO₂ / acetic acid / 3 h / Ambient temperature

With hydrogen; platinum(IV) oxide; In pyridine; acetic acid;
DOI:10.1021/jo00316a021

Reference yield:

: 21090-30-2
3'-O-acetylthymidine

: 75863-44-4
3-O-acetyl-1,2,5,6-tetradeoxy-1-<3-(4-toluyl)thymin-1-yl)>-β-D-erythro-heptafuranuronic acid

Guidance literature:: Multi-step reaction with 5 steps

2: Dowex 5OW-X₈(H(+)) / H₂O; tetrahydrofuran / 6 h

3: 54 percent / acetonitrile / 20 h / Ambient temperature

4: pyridine / 1) 1h, cold, 2) 40h at ambient temp.

5: 93 percent / H₂ / PtO₂ / acetic acid / 3 h / Ambient temperature

With Dowex 5OW-X₈(H(+)); hydrogen; platinum(IV) oxide; In tetrahydrofuran; pyridine; water; acetic acid; acetonitrile;
DOI:10.1021/jo00316a021