methyl 4-(4-methyl-N-(3-methylbut-2-enyl)phenylsulfonamido)-1-phenylbut-2-ynyl carbonate

Base Information

Chemical Name:methyl 4-(4-methyl-N-(3-methylbut-2-enyl)phenylsulfonamido)-1-phenylbut-2-ynyl carbonate
CAS No.:1363388-19-5
Molecular Formula:C₂₄H₂₇NO₅S
Molecular Weight:441.548
Hs Code.:

Synonyms:methyl 4-(4-methyl-N-(3-methylbut-2-enyl)phenylsulfonamido)-1-phenylbut-2-ynyl carbonate

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Chemical Property of methyl 4-(4-methyl-N-(3-methylbut-2-enyl)phenylsulfonamido)-1-phenylbut-2-ynyl carbonate

Chemical Property:

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Technology Process of methyl 4-(4-methyl-N-(3-methylbut-2-enyl)phenylsulfonamido)-1-phenylbut-2-ynyl carbonate

There total 3 articles about methyl 4-(4-methyl-N-(3-methylbut-2-enyl)phenylsulfonamido)-1-phenylbut-2-ynyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1174503-07-1
C₂₂H₂₅NO₃S

: 79-22-1
methyl chloroformate

: 1363388-19-5
methyl 4-(4-methyl-N-(3-methylbut-2-enyl)phenylsulfonamido)-1-phenylbut-2-ynyl carbonate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 2.5h;
DOI:10.1021/jo202590w

Reference yield:

: 132330-44-0
N-prenyl-N-propargyltosylamide

: 1363388-19-5
methyl 4-(4-methyl-N-(3-methylbut-2-enyl)phenylsulfonamido)-1-phenylbut-2-ynyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethylmagnesium bromide / tetrahydrofuran / 1 h / 50 °C

1.2: 3 h / 20 °C

2.1: pyridine / dichloromethane / 2.5 h / 0 °C

With pyridine; ethylmagnesium bromide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo202590w

Reference yield:

: 100-52-7
benzaldehyde

: 1363388-19-5
methyl 4-(4-methyl-N-(3-methylbut-2-enyl)phenylsulfonamido)-1-phenylbut-2-ynyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethylmagnesium bromide / tetrahydrofuran / 1 h / 50 °C

1.2: 3 h / 20 °C

2.1: pyridine / dichloromethane / 2.5 h / 0 °C

With pyridine; ethylmagnesium bromide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo202590w