(2S-cis)-N-methyl-2-(2-methyl-1-propenyl)-4,N-diphenyl-3-oxazolidinecarboxamide

Base Information

Chemical Name:(2S-cis)-N-methyl-2-(2-methyl-1-propenyl)-4,N-diphenyl-3-oxazolidinecarboxamide
CAS No.:298210-08-9
Molecular Formula:C₂₁H₂₄N₂O₂
Molecular Weight:336.434
Hs Code.:

Synonyms:(2S-cis)-N-methyl-2-(2-methyl-1-propenyl)-4,N-diphenyl-3-oxazolidinecarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S-cis)-N-methyl-2-(2-methyl-1-propenyl)-4,N-diphenyl-3-oxazolidinecarboxamide

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Technology Process of (2S-cis)-N-methyl-2-(2-methyl-1-propenyl)-4,N-diphenyl-3-oxazolidinecarboxamide

There total 4 articles about (2S-cis)-N-methyl-2-(2-methyl-1-propenyl)-4,N-diphenyl-3-oxazolidinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 298210-06-7
(2S-cis)-2-(2-methyl-1-propenyl)-4,N-diphenyl-3-oxazolidinecarboxamide

: 74-88-4
methyl iodide

: 298210-08-9
(2S-cis)-N-methyl-2-(2-methyl-1-propenyl)-4,N-diphenyl-3-oxazolidinecarboxamide

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; at 20 ℃;
DOI:10.1021/ja001113l

Reference yield:

: 107-86-8
3,3-dimethyl acrylaldehyde

: 298210-08-9
(2S-cis)-N-methyl-2-(2-methyl-1-propenyl)-4,N-diphenyl-3-oxazolidinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: molecular sieves 4 Angstroem / CH₂Cl₂ / 3 h / 20 °C

2: 1.78 g / CH₂Cl₂; diethyl ether / 16 h / 20 °C

3: 41 percent / potassium hydroxide / dimethylsulfoxide / 20 °C

With potassium hydroxide; 4 A molecular sieve; In diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja010463k

Reference yield:

: 20989-17-7
(2S)-2-phenylglycinol

: 298210-08-9
(2S-cis)-N-methyl-2-(2-methyl-1-propenyl)-4,N-diphenyl-3-oxazolidinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: molecular sieves 4 Angstroem / CH₂Cl₂ / 3 h / 20 °C

2: 1.78 g / CH₂Cl₂; diethyl ether / 16 h / 20 °C

3: 41 percent / potassium hydroxide / dimethylsulfoxide / 20 °C

With potassium hydroxide; 4 A molecular sieve; In diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja010463k