Technology Process of (2-(diethoxymethyl)phenyl)(methyl)tellane
There total 4 articles about (2-(diethoxymethyl)phenyl)(methyl)tellane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1,2-bis(2-(diethoxymethyl)phenyl)ditellane;
With
sodium tetrahydroborate; ethanol;
at 20 ℃;
for 0.5h;
Inert atmosphere;
methyl iodide;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/acsmedchemlett.8b00362
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ethanol / Inert atmosphere; Reflux
2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
2.2: 2 h / 20 °C / Inert atmosphere
3.1: sodium tetrahydroborate; ethanol / 0.5 h / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
With
sodium tetrahydroborate; n-butyllithium; ethanol;
In
tetrahydrofuran; ethanol;
DOI:10.1021/acsmedchemlett.8b00362
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
1.2: 2 h / 20 °C / Inert atmosphere
2.1: sodium tetrahydroborate; ethanol / 0.5 h / 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
With
sodium tetrahydroborate; n-butyllithium; ethanol;
In
tetrahydrofuran;
DOI:10.1021/acsmedchemlett.8b00362
