C₅₅H₅₁Cl₃N₄O₁₃

Base Information

• Chemical Name: C₅₅H₅₁Cl₃N₄O₁₃
• CAS No.: 657395-03-4
• Molecular Formula: C₅₅H₅₁Cl₃N₄O₁₃
• Molecular Weight: 1082.39
• Mol file: 657395-03-4.mol

Synonyms:C₅₅H₅₁Cl₃N₄O₁₃

Chemical Property of C₅₅H₅₁Cl₃N₄O₁₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₅H₅₁Cl₃N₄O₁₃

There total 19 articles about C₅₅H₅₁Cl₃N₄O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-O-benzyl-1,6-anhydro-β-L-idopyranose (42926-91-0) → C55H51Cl3N4O13 (657395-03-4)

Guidance literature:

Multi-step reaction with 5 steps

1: 85 percent / pyridine

2: 61 percent / TMSOTf

3: 88 percent / Cu(OTf)2

4: NH₃(g)

5: DBU

With pyridine; trimethylsilyl trifluoromethanesulfonate; ammonia; copper(II) bis(trifluoromethanesulfonate); 1,8-diazabicyclo[5.4.0]undec-7-ene;

DOI:10.1002/jccs.200400175

Reference yield:

1,6-anhydro-2-O-benzoyl-3-O-benzyl-β-L-idopyranoside (334834-19-4) → C55H51Cl3N4O13 (657395-03-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 61 percent / TMSOTf

2: 88 percent / Cu(OTf)2

3: NH₃(g)

4: DBU

With trimethylsilyl trifluoromethanesulfonate; ammonia; copper(II) bis(trifluoromethanesulfonate); 1,8-diazabicyclo[5.4.0]undec-7-ene;

DOI:10.1002/jccs.200400175

Reference yield:

(2R,4aR,7R,8R,8aS)-7-Azido-2-naphthalen-2-yl-hexahydro-pyrano[3,2-d][1,3]dioxine-6,8-diol → C55H51Cl3N4O13 (657395-03-4)

Guidance literature:

Multi-step reaction with 10 steps

1: Et₃N

2: Ag₂O

3: 84 percent / VO(OTf)2; BH₃ / tetrahydrofuran

4: 90 percent / pyridine

5: 96 percent / NH₃(g)

6: 98 percent / K₂CO₃

7: 61 percent / TMSOTf

8: 88 percent / Cu(OTf)2

9: NH₃(g)

10: DBU

With pyridine; vanadyl triflate; trimethylsilyl trifluoromethanesulfonate; borane; ammonia; copper(II) bis(trifluoromethanesulfonate); potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; silver(l) oxide; In tetrahydrofuran;

DOI:10.1002/jccs.200400175

upstream raw materials:

trichloroacetonitrile

6-hydroxy-1,2:3,5-di-O-isopropylidene-α-D-glucofuranoside

6-deoxy-1,2:3,5-di-O-isopropylidene-α-D-xylo-hex-5-enofuranose

1,6-anhydro-β-L-idopyranose

Downstream raw materials:

C₇₄H₇₂N₆O₁₈