ethyl 2,3,6-tri-O-benzyl-4-O-(N,N-diethylthiocarbamoyl)-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:ethyl 2,3,6-tri-O-benzyl-4-O-(N,N-diethylthiocarbamoyl)-1-thio-α-D-mannopyranoside
CAS No.:850873-44-8
Molecular Formula:C₃₄H₄₃NO₅S₂
Molecular Weight:609.851
Hs Code.:

Synonyms:ethyl 2,3,6-tri-O-benzyl-4-O-(N,N-diethylthiocarbamoyl)-1-thio-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2,3,6-tri-O-benzyl-4-O-(N,N-diethylthiocarbamoyl)-1-thio-α-D-mannopyranoside

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Technology Process of ethyl 2,3,6-tri-O-benzyl-4-O-(N,N-diethylthiocarbamoyl)-1-thio-α-D-mannopyranoside

There total 1 articles about ethyl 2,3,6-tri-O-benzyl-4-O-(N,N-diethylthiocarbamoyl)-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 88-11-9
N,N-diethylthiocarbamoyl chloride

: 152964-79-9
ethyl 2,3,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

: 850873-44-8
ethyl 2,3,6-tri-O-benzyl-4-O-(N,N-diethylthiocarbamoyl)-1-thio-α-D-mannopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 16h;
DOI:10.1002/ejoc.200400616

Reference yield: 49.0%

: 850873-44-8
ethyl 2,3,6-tri-O-benzyl-4-O-(N,N-diethylthiocarbamoyl)-1-thio-α-D-mannopyranoside

: 2382-96-9,118090-08-7
2-sulfanyl-1,3-benzoxazole

: 850873-46-0
benzoxazolyl 2,3,6-tri-O-benzyl-4-O-(N,N-diethylthiocarbamoyl)-1-thio-α-D-mannopyranoside

Guidance literature:: With iodonium(di-γ-collidine) perchlorate; 4 A molecular sieve; In dichloromethane; at 0 - 20 ℃; for 24h;
DOI:10.1002/ejoc.200400616

Reference yield:

: 850873-44-8
ethyl 2,3,6-tri-O-benzyl-4-O-(N,N-diethylthiocarbamoyl)-1-thio-α-D-mannopyranoside

: 53182-61-9
methyl 2,3,4-tri-O-benzoyl-β-D-galactopyranoside

: C₆₀H₆₃NO₁₄S

: C₆₀H₆₃NO₁₄S

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 20 ℃; Further Variations:; Temperatures; Product distribution;
DOI:10.1002/ejoc.200400616