Xanthyliden-⁽⁹⁾-acetophenon

Base Information

Chemical Name:Xanthyliden-⁽⁹⁾-acetophenon
CAS No.:102183-97-1
Molecular Formula:C₂₁H₁₄O₂
Molecular Weight:298.341
Hs Code.:

Synonyms:Xanthyliden-⁽⁹⁾-acetophenon

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Xanthyliden-⁽⁹⁾-acetophenon

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Technology Process of Xanthyliden-⁽⁹⁾-acetophenon

There total 3 articles about Xanthyliden-⁽⁹⁾-acetophenon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 492-21-7
9H-xanthene-9-thione

: 3282-32-4
2-diazo-acetophenone

: 102183-97-1
Xanthyliden-⁽⁹⁾-acetophenon

Guidance literature:: In tetrahydrofuran; at 65 ℃; for 20h;
DOI:10.1002/hlca.19960790327

Reference yield:

: 28447-91-8
9-chloro-9H-xanthene

: 70-11-1
α-bromoacetophenone

: 102183-97-1
Xanthyliden-⁽⁹⁾-acetophenon

Guidance literature:: With 1,2,3-Benzotriazole; n-butyllithium; Yield given. Multistep reaction; 2.) THF, cyclohexane, -78 deg C, 30 min, 3.) THF, -78 deg C, 2 h; room temperature, 10 h;
DOI:10.1021/jo9800199