cis-3-acetoxy-4-(oxy)-2-(<(1α,2β,6β)-2,6-bis(phenylmethoxy)-1-cyclohexyl>oxy)-6-methyl-5,6-dihydro-2H-pyran

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Chemical Name:cis-3-acetoxy-4-(oxy)-2-(<(1α,2β,6β)-2,6-bis(phenylmethoxy)-1-cyclohexyl>oxy)-6-methyl-5,6-dihydro-2H-pyran
CAS No.:102922-64-5
Molecular Formula:C₃₄H₄₈O₇Si
Molecular Weight:596.836
Hs Code.:

cis-3-acetoxy-4-(<dimethyl(1,1-dimethylethyl)silyl>oxy)-2-(<(1α,2β,6β)-2,6-bis(phenylmethoxy)-1-cyclohexyl>oxy)-6-methyl-5,6-dihydro-2H-pyran

Synonyms:cis-3-acetoxy-4-(oxy)-2-(<(1α,2β,6β)-2,6-bis(phenylmethoxy)-1-cyclohexyl>oxy)-6-methyl-5,6-dihydro-2H-pyran

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Chemical Property of cis-3-acetoxy-4-(oxy)-2-(<(1α,2β,6β)-2,6-bis(phenylmethoxy)-1-cyclohexyl>oxy)-6-methyl-5,6-dihydro-2H-pyran

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Technology Process of cis-3-acetoxy-4-(oxy)-2-(<(1α,2β,6β)-2,6-bis(phenylmethoxy)-1-cyclohexyl>oxy)-6-methyl-5,6-dihydro-2H-pyran

There total 7 articles about cis-3-acetoxy-4-(oxy)-2-(<(1α,2β,6β)-2,6-bis(phenylmethoxy)-1-cyclohexyl>oxy)-6-methyl-5,6-dihydro-2H-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 75-07-0,9002-91-9
acetaldehyde

: 102922-68-9
Acetic acid 1-[1-((1R,2S,6R)-2,6-bis-benzyloxy-cyclohexyloxy)-meth-(Z)-ylidene]-2-(tert-butyl-dimethyl-silanyloxy)-allyl ester

: 102922-64-5
cis-3-acetoxy-4-(oxy)-2-(<(1α,2β,6β)-2,6-bis(phenylmethoxy)-1-cyclohexyl>oxy)-6-methyl-5,6-dihydro-2H-pyran

Guidance literature:: In chloroform-d1; for 36h; Ambient temperature;
DOI:10.1021/ja00274a049

Reference yield:

: 74441-37-5
2-acetoxy-1-methoxy-1-buten-3-one

: 102922-64-5
cis-3-acetoxy-4-(oxy)-2-(<(1α,2β,6β)-2,6-bis(phenylmethoxy)-1-cyclohexyl>oxy)-6-methyl-5,6-dihydro-2H-pyran

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / benzene / 20 h / Heating

2: 99 percent / triethylamine / diethyl ether / 0.17 h / 0 °C

3: 51 percent / CDCl₃ / 36 h / Ambient temperature

With triethylamine; In diethyl ether; chloroform-d1; benzene;
DOI:10.1021/ja00274a049

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 102922-64-5
cis-3-acetoxy-4-(oxy)-2-(<(1α,2β,6β)-2,6-bis(phenylmethoxy)-1-cyclohexyl>oxy)-6-methyl-5,6-dihydro-2H-pyran

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / triethylamine / diethyl ether / 0.17 h / 0 °C

2: 51 percent / CDCl₃ / 36 h / Ambient temperature

With triethylamine; In diethyl ether; chloroform-d1;
DOI:10.1021/ja00274a049