Technology Process of 2-ethyl-3-methylbutyl phenyl sulphone
There total 5 articles about 2-ethyl-3-methylbutyl phenyl sulphone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
chloroform;
for 2h;
Ambient temperature;
DOI:10.1007/BF00629972
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) BuLi, diisopropylamine, hexamethylphosphorotriamide / 1.) THF, hexane, -5 deg C, 30 min, 2.) THF, RT, 2 h
2: 50 percent / LiAlH4 / diethyl ether / 1 h
3: 3.3 g / pyridine / 2 h
4: 80 percent / NaOMe / methanol / 10 h / Ambient temperature
5: 95 percent / m-chloroperbenzoic acid / CHCl3 / 2 h / Ambient temperature
With
pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; n-butyllithium; sodium methylate; diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
methanol; diethyl ether; chloroform;
DOI:10.1007/BF00629972
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 50 percent / LiAlH4 / diethyl ether / 1 h
2: 3.3 g / pyridine / 2 h
3: 80 percent / NaOMe / methanol / 10 h / Ambient temperature
4: 95 percent / m-chloroperbenzoic acid / CHCl3 / 2 h / Ambient temperature
With
pyridine; lithium aluminium tetrahydride; sodium methylate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; diethyl ether; chloroform;
DOI:10.1007/BF00629972
