Technology Process of 2-ethyl-3-methylbutyl phenyl sulfide
There total 4 articles about 2-ethyl-3-methylbutyl phenyl sulfide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium methylate;
In
methanol;
for 10h;
Ambient temperature;
DOI:10.1007/BF00629972
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) BuLi, diisopropylamine, hexamethylphosphorotriamide / 1.) THF, hexane, -5 deg C, 30 min, 2.) THF, RT, 2 h
2: 50 percent / LiAlH4 / diethyl ether / 1 h
3: 3.3 g / pyridine / 2 h
4: 80 percent / NaOMe / methanol / 10 h / Ambient temperature
With
pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; n-butyllithium; sodium methylate; diisopropylamine;
In
methanol; diethyl ether;
DOI:10.1007/BF00629972
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 50 percent / LiAlH4 / diethyl ether / 1 h
2: 3.3 g / pyridine / 2 h
3: 80 percent / NaOMe / methanol / 10 h / Ambient temperature
With
pyridine; lithium aluminium tetrahydride; sodium methylate;
In
methanol; diethyl ether;
DOI:10.1007/BF00629972
