N-{4-[(2,3-dihydroxyphenyl)formamido]butyl}-2,3-dihydroxybenzamide

Base Information

• Chemical Name: N-{4-[(2,3-dihydroxyphenyl)formamido]butyl}-2,3-dihydroxybenzamide
• CAS No.: 71636-73-2
• Molecular Formula: C₁₈H₂₀N₂O₆
• Molecular Weight: 360.367
• Mol file: 71636-73-2.mol

Synonyms:N-{4-[(2,3-dihydroxyphenyl)formamido]butyl}-2,3-dihydroxybenzamide

Chemical Property of N-{4-[(2,3-dihydroxyphenyl)formamido]butyl}-2,3-dihydroxybenzamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-{4-[(2,3-dihydroxyphenyl)formamido]butyl}-2,3-dihydroxybenzamide

There total 5 articles about N-{4-[(2,3-dihydroxyphenyl)formamido]butyl}-2,3-dihydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N,N'-bis(2,3-dimethoxybenzoyl)-1,4-diaminobutane (73630-96-3) → N-{4-[(2,3-dihydroxyphenyl)formamido]butyl}-2,3-dihydroxybenzamide (71636-73-2)

Guidance literature:

With boron tribromide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.ejmech.2015.01.033

Reference yield: 95.0%

2,3-bis(benzyloxy)-N-(4-{[2,3-bis(benzyloxy)phenyl]formamido}butyl)benzamide → N-{4-[(2,3-dihydroxyphenyl)formamido]butyl}-2,3-dihydroxybenzamide (71636-73-2)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; toluene; for 18h;

DOI:10.1002/anie.201300751

Reference yield: 45.0%

chlorure de 2,3-dioxosulfinylbenzoyle (70656-95-0) + 1,4-diaminobutane (110-60-1) → N-{4-[(2,3-dihydroxyphenyl)formamido]butyl}-2,3-dihydroxybenzamide (71636-73-2)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; for 12h; Heating;

DOI:10.1002/jps.2600690836

upstream raw materials:

N,N'-bis(2,3-dimethoxybenzoyl)-1,4-diaminobutane

chlorure de 2,3-dioxosulfinylbenzoyle

1,4-diaminobutane

2,3-dimethoxybenzoic acid

Downstream raw materials:

N,N'-bis(2,3-dihydroxy-5-sulfobenzoyl)-1,6-diazahexane