N-(2-methylprop-2-enyl)benzylamide

Base Information

• Chemical Name: N-(2-methylprop-2-enyl)benzylamide
• CAS No.: 128863-85-4
• Molecular Formula: C₁₂H₁₅NO
• Molecular Weight: 189.257
• Mol file: 128863-85-4.mol

Synonyms:N-(2-methylprop-2-enyl)benzylamide

Chemical Property of N-(2-methylprop-2-enyl)benzylamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N-(2-methylprop-2-enyl)benzylamide

There total 4 articles about N-(2-methylprop-2-enyl)benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

N-benzyloyl-2,2-dimethylaziridine → N-(2-methylprop-2-enyl)benzylamide (128863-85-4) + N-(2-hydroxy-2-methylpropyl)benzylamide + 2-benzyl-5,5-dimethyloxazoline (106013-39-2)

Guidance literature:

With sulfuric acid; water; In diethyl ether; at 20 ℃; for 96h; Mechanism; Cooling;

DOI:10.1007/s12039-015-1020-x

Reference yield:

phenylacetyl chloride (103-80-0) → N-(2-methylprop-2-enyl)benzylamide (128863-85-4) + N-(2-hydroxy-2-methylpropyl)benzylamide

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / benzene

2: water; sulfuric acid / diethyl ether / 96 h / 20 °C / Cooling

With sulfuric acid; water; triethylamine; In diethyl ether; benzene;

DOI:10.1007/s12039-015-1020-x

Reference yield:

Benzeneacetamide (103-81-1) → N-(2-methylprop-2-enyl)benzylamide (128863-85-4)

Guidance literature:

With 1,4-dioxane; potassium; anschliessendes Erhitzen mit Methallylchlorid;

upstream raw materials:

Benzeneacetamide

phenylacetyl chloride

Downstream raw materials:

2-methyl-2-propen-1-yl phenylacetate