((R)-2-acetylsulfanyl-4-oxo-azetidin-1-yl)-(triphenyl-λ⁵-phosphanylidene)-acetic acid 4-nitro-benzyl ester

Base Information

• Chemical Name: ((R)-2-acetylsulfanyl-4-oxo-azetidin-1-yl)-(triphenyl-λ⁵-phosphanylidene)-acetic acid 4-nitro-benzyl ester
• CAS No.: 69126-87-0
• Molecular Formula: C₃₂H₂₇N₂O₆PS
• Molecular Weight: 598.616

Synonyms:((R)-2-acetylsulfanyl-4-oxo-azetidin-1-yl)-(triphenyl-λ⁵-phosphanylidene)-acetic acid 4-nitro-benzyl ester

Chemical Property of ((R)-2-acetylsulfanyl-4-oxo-azetidin-1-yl)-(triphenyl-λ⁵-phosphanylidene)-acetic acid 4-nitro-benzyl ester

Chemical Property:

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Technology Process of ((R)-2-acetylsulfanyl-4-oxo-azetidin-1-yl)-(triphenyl-λ⁵-phosphanylidene)-acetic acid 4-nitro-benzyl ester

There total 1 articles about ((R)-2-acetylsulfanyl-4-oxo-azetidin-1-yl)-(triphenyl-λ⁵-phosphanylidene)-acetic acid 4-nitro-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ ((R)-2-acetylsulfanyl-4-oxo-azetidin-1-yl)-(triphenyl-λ5-phosphanylidene)-acetic acid 4-nitro-benzyl ester (69126-87-0)

Guidance literature:

Chlorid 15, Triphenylphosphin;

DOI:10.1021/ja00515a025

Reference yield:

((R)-2-acetylsulfanyl-4-oxo-azetidin-1-yl)-(triphenyl-λ5-phosphanylidene)-acetic acid 4-nitro-benzyl ester (69126-87-0) → (R)-3-methyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitro-benzyl ester (69126-88-1)

Guidance literature:

With hydroquinone; In toluene; at 90 ℃; for 40h;

DOI:10.1021/ja00515a025

Reference yield:

((R)-2-acetylsulfanyl-4-oxo-azetidin-1-yl)-(triphenyl-λ5-phosphanylidene)-acetic acid 4-nitro-benzyl ester (69126-87-0) → 3-methyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitro-benzyl ester (72597-68-3)

Guidance literature:

hydroquinone; In toluene;

Downstream raw materials:

(R)-3-methyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitro-benzyl ester

3-methyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitro-benzyl ester

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