C₂₂H₂₉NO₉

Base Information

• Chemical Name: C₂₂H₂₉NO₉
• CAS No.: 946428-55-3
• Molecular Formula: C₂₂H₂₉NO₉
• Molecular Weight: 451.474
• Mol file: 946428-55-3.mol

Synonyms:C₂₂H₂₉NO₉

Chemical Property of C₂₂H₂₉NO₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₉NO₉

There total 8 articles about C₂₂H₂₉NO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H27NO9 (946428-54-2) → C22H29NO9 (946428-55-3)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethanol; under 3620.13 Torr;

DOI:10.1021/ol070980t

Reference yield:

N-carbomethoxy-L-3-dehydroproline methyl ester → C22H29NO9 (946428-55-3)

Guidance literature:

Multi-step reaction with 5 steps

1.1: aq. AcOH / Pd(OAc)2 / acetonitrile / 4 h / 60 °C

1.2: 65 percent / 2,4-lutidine; trifluoroacetic anhydride / toluene

2.1: NaH / tetrahydrofuran / 0 - 20 °C

2.2: 79 percent / tetrahydrofuran

3.1: LiHMDS / tetrahydrofuran / 0.5 h / 0 °C

3.2: 72 percent / tetrahydrofuran / 18 h / 0 - 20 °C

4.1: H₂O₂ / tetrahydrofuran / 0 - 20 °C

5.1: H₂ / PtO₂ / ethanol / 3620.13 Torr

With hydrogen; dihydrogen peroxide; sodium hydride; acetic acid; lithium hexamethyldisilazane; platinum(IV) oxide; palladium diacetate; In tetrahydrofuran; ethanol; acetonitrile; 2.2: Michael reaction;

DOI:10.1021/ol070980t

Reference yield:

2-methoxyphenyldiazonium tetrafluoroborate (492-95-5) → C22H29NO9 (946428-55-3)

Guidance literature:

Multi-step reaction with 5 steps

1.1: aq. AcOH / Pd(OAc)2 / acetonitrile / 4 h / 60 °C

1.2: 65 percent / 2,4-lutidine; trifluoroacetic anhydride / toluene

2.1: NaH / tetrahydrofuran / 0 - 20 °C

2.2: 79 percent / tetrahydrofuran

3.1: LiHMDS / tetrahydrofuran / 0.5 h / 0 °C

3.2: 72 percent / tetrahydrofuran / 18 h / 0 - 20 °C

4.1: H₂O₂ / tetrahydrofuran / 0 - 20 °C

5.1: H₂ / PtO₂ / ethanol / 3620.13 Torr

With hydrogen; dihydrogen peroxide; sodium hydride; acetic acid; lithium hexamethyldisilazane; platinum(IV) oxide; palladium diacetate; In tetrahydrofuran; ethanol; acetonitrile; 2.2: Michael reaction;

DOI:10.1021/ol070980t

upstream raw materials:

C₂₂H₂₇NO₉

C₁₆H₂₁NO₆

4-(o-methoxyphenyl)dehydroproline

C₂₂H₂₉NO₉

Downstream raw materials:

C₁₆H₁₉NO₇

C₂₄H₂₇NO₇

C₁₄H₁₇NO₅