[(η5-pentamethylcyclopentadienyl)2Rh2(μ-I)2(CH2CH2CF(CF3)2)2]*benzene-d6

Base Information

Chemical Name:[(η5-pentamethylcyclopentadienyl)2Rh2(μ-I)2(CH2CH2CF(CF3)2)2]*benzene-d6
CAS No.:1350458-19-3
Molecular Formula:C₆H₆*C₃₀H₃₈F₁₄I₂Rh₂
Molecular Weight:1208.3
Hs Code.:

Synonyms:[(η5-pentamethylcyclopentadienyl)2Rh2(μ-I)2(CH2CH2CF(CF3)2)2]*benzene-d6

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Chemical Property of [(η5-pentamethylcyclopentadienyl)2Rh2(μ-I)2(CH2CH2CF(CF3)2)2]*benzene-d6

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Technology Process of [(η5-pentamethylcyclopentadienyl)2Rh2(μ-I)2(CH2CH2CF(CF3)2)2]*benzene-d6

There total 1 articles about [(η5-pentamethylcyclopentadienyl)2Rh2(μ-I)2(CH2CH2CF(CF3)2)2]*benzene-d6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32613-78-8
Cp*Rh(ethylene)2

: 677-69-0
perfluoroisopropyl iodide

: 1349736-92-0
[(η5-pentamethylcyclopentadienyl)2Rh2I(μ-I)2(CH2CH2CF(CF3)2)]

: 1350458-19-3
[(η5-pentamethylcyclopentadienyl)2Rh2(μ-I)2(CH2CH2CF(CF3)2)2]*benzene-d6

Guidance literature:: In pentane; byproducts: CH2CH2; (N2, Schlenk technique); addn. of perfluoroisopropyl iodide to pentane soln. of rhodium compd., stirring at room temp. for 18 h; filtration, washing with pentane, drying in vac., NMR and elem. anal.;
DOI:10.1021/om2009588

Reference yield: 86.0%

: 1349736-92-0
[(η5-pentamethylcyclopentadienyl)2Rh2I(μ-I)2(CH2CH2CF(CF3)2)]

: 1350458-19-3
[(η5-pentamethylcyclopentadienyl)2Rh2(μ-I)2(CH2CH2CF(CF3)2)2]*benzene-d6

: 603-35-0
triphenylphosphine

: 754-34-7
1,1,1,2,2,3,3-heptafluoro-3-iodo-propane

: 1349737-19-4
[(η5-pentamethylcyclopentadienyl)RhI(CH2CH2CF(CF3)2)(PPh3)]

Guidance literature:: In tetrahydrofuran; byproducts: CH2CH2; (N2, Schlenk technique); stirring mixt. of rhodium compds. and phosphinederiv. in THF for 5 h; evapn. in vac., chromy. (silica gel, diethyl ether/hexane (1:1)), evapn., elem. anal.;
DOI:10.1021/om2009588