methyl (2S)-(4-methoxycarbonylphenoxy)-3-phenylpropionate

Base Information

Chemical Name:methyl (2S)-(4-methoxycarbonylphenoxy)-3-phenylpropionate
CAS No.:142696-19-3
Molecular Formula:C₁₈H₁₈O₅
Molecular Weight:314.338
Hs Code.:

Synonyms:methyl (2S)-(4-methoxycarbonylphenoxy)-3-phenylpropionate

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Chemical Property of methyl (2S)-(4-methoxycarbonylphenoxy)-3-phenylpropionate

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Technology Process of methyl (2S)-(4-methoxycarbonylphenoxy)-3-phenylpropionate

There total 1 articles about methyl (2S)-(4-methoxycarbonylphenoxy)-3-phenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 828-01-3,7326-19-4,20312-36-1,156-05-8
D-phenyllactic acid

: 142696-19-3
methyl (2S)-(4-methoxycarbonylphenoxy)-3-phenylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / 98percent H₂SO₄ / CH₂Cl₂ / 18 h / Heating

2: 70 percent / (C₆H₅)3P, diisopropyl azodicarboxylate / tetrahydrofuran / Ambient temperature

With di-isopropyl azodicarboxylate; sulfuric acid; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/jhet.5570290223

Reference yield: 98.0%

: 142696-19-3
methyl (2S)-(4-methoxycarbonylphenoxy)-3-phenylpropionate

: 142696-21-7
(2S)-(4-methoxycarbonylphenoxy)-3-phenyl-1-propanol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; water; for 30h; Ambient temperature;
DOI:10.1002/jhet.5570290223

Reference yield:

: 142696-19-3
methyl (2S)-(4-methoxycarbonylphenoxy)-3-phenylpropionate

: 109210-00-6
(2R)-benzyl-6-(formyl)-2,3-dihydro-4H-benzopyran

Guidance literature:: Multi-step reaction with 10 steps

1: 98 percent / NaBH₄ / tetrahydrofuran; H₂O / 30 h / Ambient temperature

2: 99 percent / triphenylphosphine dibromide / CH₂Cl₂ / 28 °C

3: methanesulfonic acid / 20 °C

4: Et₃N, Ac₂O / dimethylformamide / 1 h / 37 °C

5: 4 N HCl / acetone / Ambient temperature

6: 1 M sodium hypochlorite / ethyl acetate / 4 h / Ambient temperature

7: Zn, AcOH

8: 74 percent / H₂, HCl / 10percent Pd/C / tetrahydrofuran; H₂O / 30 h / 2585.7 Torr

9: sodium bis-(2-methoxyethoxy)aluminium hydride / toluene / 1 h / 20 °C

10: 80 percent / MnO₂ / toluene / 2 h

With hydrogenchloride; manganese(IV) oxide; sodium hypochlorite; sodium tetrahydroborate; methanesulfonic acid; hydrogen; acetic anhydride; acetic acid; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; zinc; dibromotriphenylphosphorane; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1002/jhet.5570290223