Technology Process of C26H43N5O6
There total 12 articles about C26H43N5O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 0 ℃;
for 14h;
DOI:10.1021/ja105119r
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 0 ℃;
for 14h;
DOI:10.1021/ja105119r
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane / dichloromethane / 2.75 h / -78 - -65 °C / Inert atmosphere
1.2: 3.25 h / -78 - -67 °C
2.1: water; dihydrogen peroxide; sodium hydroxide / methanol; tert-butyl alcohol / 0 - 20 °C
2.2: pH 4
3.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere
4.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
5.1: dimethylsulfide borane complex / tetrahydrofuran / 5 h / 65 °C / Inert atmosphere
6.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C
7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 0 °C
With
2,6-dimethylpyridine; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; dihydrogen peroxide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane;
In
tetrahydrofuran; methanol; dichloromethane; tert-butyl alcohol;
DOI:10.1021/ja105119r
