phosphoric acid (4R,5S)-[5-⁽²⁾H]-5-acetyl-2,2-dimethyl-1,3-dioxolan-4-ylmethyl ester dibenzyl ester

Base Information

• Chemical Name: phosphoric acid (4R,5S)-[5-⁽²⁾H]-5-acetyl-2,2-dimethyl-1,3-dioxolan-4-ylmethyl ester dibenzyl ester
• CAS No.: 247600-25-5
• Molecular Formula: C₂₂H₂₇O₇P
• Molecular Weight: 435.418

Synonyms:phosphoric acid (4R,5S)-[5-⁽²⁾H]-5-acetyl-2,2-dimethyl-1,3-dioxolan-4-ylmethyl ester dibenzyl ester

Chemical Property of phosphoric acid (4R,5S)-[5-⁽²⁾H]-5-acetyl-2,2-dimethyl-1,3-dioxolan-4-ylmethyl ester dibenzyl ester

Chemical Property:

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Technology Process of phosphoric acid (4R,5S)-[5-⁽²⁾H]-5-acetyl-2,2-dimethyl-1,3-dioxolan-4-ylmethyl ester dibenzyl ester

There total 5 articles about phosphoric acid (4R,5S)-[5-⁽²⁾H]-5-acetyl-2,2-dimethyl-1,3-dioxolan-4-ylmethyl ester dibenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-((4'S,5'R)-[4'-(2)H]-5'-benzyloxymethyl-2',2'-dimethyl-1',3'-dioxolan-4'-yl)-ethanone → phosphoric acid (4R,5S)-[5-(2)H]-5-acetyl-2,2-dimethyl-1,3-dioxolan-4-ylmethyl ester dibenzyl ester (247600-25-5)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogen / Pd/C / ethanol

2: tetrazole

3: t-BuOOH / CH₂Cl₂

With 1H-tetrazole; tert.-butylhydroperoxide; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane;

DOI:10.1021/ol990839n

Reference yield:

2,2-dimethoxy-propane (77-76-9) → phosphoric acid (4R,5S)-[5-(2)H]-5-acetyl-2,2-dimethyl-1,3-dioxolan-4-ylmethyl ester dibenzyl ester (247600-25-5)

Guidance literature:

Multi-step reaction with 4 steps

1: p-toluenesulfonic acid / tetrahydrofuran

2: hydrogen / Pd/C / ethanol

3: tetrazole

4: t-BuOOH / CH₂Cl₂

With 1H-tetrazole; tert.-butylhydroperoxide; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;

DOI:10.1021/ol990839n

Reference yield:

C8(2)HH12O4P(OC7H7)2 → phosphoric acid (4R,5S)-[5-(2)H]-5-acetyl-2,2-dimethyl-1,3-dioxolan-4-ylmethyl ester dibenzyl ester (247600-25-5)

Guidance literature:

With tert.-butylhydroperoxide; In dichloromethane;

DOI:10.1021/ol990839n

upstream raw materials:

C₈⁽²⁾HH₁₃O₄

Dibenzyl N,N-diisopropylphosphoramidite

2,2-dimethoxy-propane

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