C₁₄H₁₂O₂S

Base Information

• Chemical Name: C₁₄H₁₂O₂S
• CAS No.: 1207472-18-1
• Molecular Formula: C₁₄H₁₂O₂S
• Molecular Weight: 244.314
• Mol file: 1207472-18-1.mol

Synonyms:C₁₄H₁₂O₂S

Chemical Property of C₁₄H₁₂O₂S

Chemical Property:

Purity/Quality:

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Technology Process of C₁₄H₁₂O₂S

There total 1 articles about C₁₄H₁₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Thiosalicylic acid (147-93-3) + 2-methoxyphenyllithium (31600-86-9) → C14H12O2S (1207472-18-1)

Guidance literature:

Thiosalicylic acid; With lithium hydride; In tetrahydrofuran; for 0.75h; Inert atmosphere; Reflux;

2-methoxyphenyllithium; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol9028447

Reference yield:

C14H12O2S (1207472-18-1) → C14H11NO3S

Guidance literature:

With isopentyl nitrite; In tetrahydrofuran; at 0 ℃; for 0.0833333h; Inert atmosphere;

DOI:10.1021/ol9028447

upstream raw materials:

Thiosalicylic acid

2-methoxyphenyllithium