N-[4-(3-anthracen-9-ylpropoxy)-2-(2,2-methoxyethyl)phenyl]-4-bromobenzamide

Base Information

Chemical Name:N-[4-(3-anthracen-9-ylpropoxy)-2-(2,2-methoxyethyl)phenyl]-4-bromobenzamide
CAS No.:556809-46-2
Molecular Formula:C₃₄H₃₂BrNO₄
Molecular Weight:598.536
Hs Code.:

Synonyms:N-[4-(3-anthracen-9-ylpropoxy)-2-(2,2-methoxyethyl)phenyl]-4-bromobenzamide

Suppliers and Price of N-[4-(3-anthracen-9-ylpropoxy)-2-(2,2-methoxyethyl)phenyl]-4-bromobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[4-(3-anthracen-9-ylpropoxy)-2-(2,2-methoxyethyl)phenyl]-4-bromobenzamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-[4-(3-anthracen-9-ylpropoxy)-2-(2,2-methoxyethyl)phenyl]-4-bromobenzamide

There total 6 articles about N-[4-(3-anthracen-9-ylpropoxy)-2-(2,2-methoxyethyl)phenyl]-4-bromobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 586-75-4
4-chlorobenzoyl chloride

: 556809-45-1
4-(3-anthracen-9-ylpropoxy)-2-(2,2-dimethoxyethyl)phenylamine

: 556809-46-2
N-[4-(3-anthracen-9-ylpropoxy)-2-(2,2-methoxyethyl)phenyl]-4-bromobenzamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1021/jo034219i

Reference yield:

: 2581-34-2,910311-23-8
3-methyl-4-nitrophenol

: 556809-46-2
N-[4-(3-anthracen-9-ylpropoxy)-2-(2,2-methoxyethyl)phenyl]-4-bromobenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: 99 percent / K₂CO₃ / dimethylformamide / 2 h / 90 °C

2.1: dimethylformamide / 16 h / Heating

2.2: 73 percent / aqueous HCl / diethyl ether / 2 h / Heating

3.1: 100 percent / p-toluenesulfonic acid / CH₂Cl₂ / 0.5 h / Heating

4.1: 74 percent / copper acetylacetonate; sodium borohydride / CH₂Cl₂; propan-2-ol; methanol / 0.5 h / Heating

5.1: 99 percent / diisopropylethylamine on polystyrene / CH₂Cl₂ / 5 h / 20 °C

With copper acetylacetonate; sodium tetrahydroborate; potassium carbonate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jo034219i

Reference yield:

: 556809-41-7
9-(3-iodopropyl)anthracene

: 556809-46-2
N-[4-(3-anthracen-9-ylpropoxy)-2-(2,2-methoxyethyl)phenyl]-4-bromobenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: 99 percent / K₂CO₃ / dimethylformamide / 2 h / 90 °C

2.1: dimethylformamide / 16 h / Heating

2.2: 73 percent / aqueous HCl / diethyl ether / 2 h / Heating

3.1: 100 percent / p-toluenesulfonic acid / CH₂Cl₂ / 0.5 h / Heating

4.1: 74 percent / copper acetylacetonate; sodium borohydride / CH₂Cl₂; propan-2-ol; methanol / 0.5 h / Heating

5.1: 99 percent / diisopropylethylamine on polystyrene / CH₂Cl₂ / 5 h / 20 °C

With copper acetylacetonate; sodium tetrahydroborate; potassium carbonate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jo034219i