6-chloro-6-deoxy-2,3-O-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose

Base Information

• Chemical Name: 6-chloro-6-deoxy-2,3-O-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose
• CAS No.: 82064-02-6
• Molecular Formula: C₁₆H₂₁ClO₇S
• Molecular Weight: 392.858

Synonyms:6-chloro-6-deoxy-2,3-O-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose

Chemical Property of 6-chloro-6-deoxy-2,3-O-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose

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Technology Process of 6-chloro-6-deoxy-2,3-O-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose

There total 1 articles about 6-chloro-6-deoxy-2,3-O-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,3-O-isopropylidene-1,6-bis-O-(p-tolylsulphonyl)-β-D-fructofuranose (32087-60-8) → 6-chloro-6-deoxy-2,3-O-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose (82064-02-6)

Guidance literature:

With N,N-dimethyl-formamide; lithium chloride; at 90 - 100 ℃; for 20h;

DOI:10.1016/S0008-6215(82)80002-5

Reference yield: 81.0%

6-chloro-6-deoxy-2,3-O-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose (82064-02-6) → 6-deoxy-2,3-O-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose (82064-03-7)

Guidance literature:

With nickel; hydrazine hydrate; barium carbonate; In ethanol; for 5h; Heating;

upstream raw materials:

2,3-O-isopropylidene-1,6-bis-O-(p-tolylsulphonyl)-β-D-fructofuranose

Downstream raw materials:

6-deoxy-2,3-O-isopropylidene-1-O-p-toluenesulfonyl-β-D-fructofuranose

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