C₁₄H₁₆N₂O₄

Base Information

Chemical Name:C₁₄H₁₆N₂O₄
CAS No.:1253798-62-7
Molecular Formula:C₁₄H₁₆N₂O₄
Molecular Weight:276.292
Hs Code.:

C<sub>14</sub>H<sub>16</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₁₄H₁₆N₂O₄

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Chemical Property of C₁₄H₁₆N₂O₄

Chemical Property:

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Technology Process of C₁₄H₁₆N₂O₄

There total 1 articles about C₁₄H₁₆N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 852821-12-6
3-benzyloxy-5-dimethylaminomethylisoxazole

: 124-38-9,18923-20-1
carbon dioxide

: 1253798-62-7
C₁₄H₁₆N₂O₄

Guidance literature:: 3-benzyloxy-5-dimethylaminomethylisoxazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -68 ℃; for 1.66667h; Inert atmosphere;

carbon dioxide; In tetrahydrofuran; hexane; for 2h;

With hydrogenchloride; In water; at 23 ℃; for 0.25h; pH=6 - 6.5;

Reference yield:

: 1253798-62-7
C₁₄H₁₆N₂O₄

: C₁₄H₁₅ClN₂O₃

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 8 - 23 ℃; for 5h; Inert atmosphere;

Reference yield:

: 1253798-62-7
C₁₄H₁₆N₂O₄

: 1373390-75-0
C₂₆H₂₉N₂O₅^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 5 h / 8 - 23 °C / Inert atmosphere

2.1: triethylamine / dmap / dichloromethane / 0 - 23 °C / Inert atmosphere

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.62 h / -78 - 20 °C / Inert atmosphere

3.2: 0.73 h / -78 - -60 °C / Inert atmosphere

With oxalyl dichloride; sodium hexamethyldisilazane; triethylamine; dmap; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; 3.1: Michael Reaction / 3.2: Michael Reaction;