O-(3'-O-acetyl-2',4'-di-O-benzyl-α-D-rhamnopyranosyl)-(1'<*>2)-1,3-di-O-benzylglycerol

Base Information

Chemical Name:O-(3'-O-acetyl-2',4'-di-O-benzyl-α-D-rhamnopyranosyl)-(1'<*>2)-1,3-di-O-benzylglycerol
CAS No.:157921-94-3
Molecular Formula:C₃₉H₄₄O₈
Molecular Weight:640.774
Hs Code.:

Synonyms:O-(3'-O-acetyl-2',4'-di-O-benzyl-α-D-rhamnopyranosyl)-(1'<*>2)-1,3-di-O-benzylglycerol

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Chemical Property of O-(3'-O-acetyl-2',4'-di-O-benzyl-α-D-rhamnopyranosyl)-(1'<*>2)-1,3-di-O-benzylglycerol

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Technology Process of O-(3'-O-acetyl-2',4'-di-O-benzyl-α-D-rhamnopyranosyl)-(1'<*>2)-1,3-di-O-benzylglycerol

There total 1 articles about O-(3'-O-acetyl-2',4'-di-O-benzyl-α-D-rhamnopyranosyl)-(1'<*>2)-1,3-di-O-benzylglycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 6972-79-8
dibenzyl glycerol

: 112612-48-3
3-O-acetyl-2,4-di-O-benzyl-α-D-rhamnopyranosyl chloride

: 157921-94-3
O-(3'-O-acetyl-2',4'-di-O-benzyl-α-D-rhamnopyranosyl)-(1'<*>2)-1,3-di-O-benzylglycerol

Guidance literature:: With 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; a) -10 deg C, 1 h, b) RT, 12 h;

Reference yield: 96.0%

: 157921-94-3
O-(3'-O-acetyl-2',4'-di-O-benzyl-α-D-rhamnopyranosyl)-(1'<*>2)-1,3-di-O-benzylglycerol

: 157921-95-4
O-(2',4'-di-O-benzyl-α-D-rhamnopyranosyl)-(1'<*>2)-1,3-di-O-benzylglycerol

Guidance literature:: With sodium methylate; In methanol; for 4h; Ambient temperature;

Reference yield:

: 157921-94-3
O-(3'-O-acetyl-2',4'-di-O-benzyl-α-D-rhamnopyranosyl)-(1'<*>2)-1,3-di-O-benzylglycerol

: 157921-96-5
O-(3-O-acetyl-2,4-di-O-benzyl-α-D-rhamnopyranosyl)-(1<*>3')-O-(2',4'-di-O-benzyl-α-D-rhamnopyranosyl)-(1'<*>2)-1,3-di-O-benzylglycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / CH₃ONa / methanol / 4 h / Ambient temperature

2: 100 mg / silver triflate, 4 A molecular sieves / CH₂Cl₂ / a) -10 deg C, 1 h, b) RT, overnight

With 4 A molecular sieve; sodium methylate; silver trifluoromethanesulfonate; In methanol; dichloromethane;