2-(AzidoMethyl)benzeneboronic acid pinacol ester, 95%

Base Information

• Chemical Name: 2-(AzidoMethyl)benzeneboronic acid pinacol ester, 95%
• CAS No.: 1223598-41-1
• Molecular Formula: C₁₃H₁₈BN₃O₂
• Molecular Weight: 259.116
• Mol file: 1223598-41-1.mol

Synonyms:2-(2-(azidomethyl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property of 2-(AzidoMethyl)benzeneboronic acid pinacol ester, 95%

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

2-(2-(Azidomethyl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane ^*data from reagent suppliers

Safty Information:

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Technology Process of 2-(AzidoMethyl)benzeneboronic acid pinacol ester, 95%

There total 5 articles about 2-(AzidoMethyl)benzeneboronic acid pinacol ester, 95% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

sodium azide + 2-(2-(bromomethyl)phenyl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane (377780-72-8) → 2-(2-(azidomethyl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1223598-41-1)

Guidance literature:

In dimethyl sulfoxide; at 20 ℃; for 16h;

DOI:10.1039/C6CC08534B

Reference yield:

2-(2-(bromomethyl)phenyl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane (377780-72-8) → 2-(2-(azidomethyl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1223598-41-1)

Guidance literature:

With sodium azide; In dimethyl sulfoxide; at 25 ℃; for 16h;

Reference yield:

2-methylphenylboronic acid pinacol ester (195062-59-0) → 2-(2-(azidomethyl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1223598-41-1)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 4 h / 90 °C

2: dimethyl sulfoxide / 16 h / 20 °C

In dimethyl sulfoxide; acetonitrile;

DOI:10.1039/C6CC08534B

upstream raw materials:

2-Methylphenylboronic acid

2,3-dimethyl-2,3-butane diol

2-methylphenylboronic acid pinacol ester

2-(2-(bromomethyl)phenyl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane

Downstream raw materials:

C₅₄H₅₆B₂N₆O₄S₈

(CH₃(CH₂)9O)2C₆H₂(CCC₆H₂(O(CH₂)9CH₃)2C₂HN₃CH₂C₆H₄B(O₂C₂(CH₃)4))2

4-phenyl-1-(2-(4,4,5,5-tetramethyl-1,3,2-dioxabololan-2-yl)benzyl)-1H-1,2,3-triazole

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