N-[4-(octa-O-acetyllactobionamidomethylene)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

Base Information

Chemical Name:N-[4-(octa-O-acetyllactobionamidomethylene)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide
CAS No.:622374-91-8
Molecular Formula:C₄₈H₆₉N₃O₂₁
Molecular Weight:1024.08
Hs Code.:

Synonyms:N-[4-(octa-O-acetyllactobionamidomethylene)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

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Chemical Property of N-[4-(octa-O-acetyllactobionamidomethylene)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

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Technology Process of N-[4-(octa-O-acetyllactobionamidomethylene)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

There total 3 articles about N-[4-(octa-O-acetyllactobionamidomethylene)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 549505-85-3
octanoic acid (2-hydroxyamino-2-methyl-propyl)-amide

: 217790-40-4
N-(4-formylbenzyl)octa-O-acetyllactobionamide

: 622374-91-8
N-[4-(octa-O-acetyllactobionamidomethylene)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

Guidance literature:: With 4 A molecular sieve; In tetrahydrofuran; at 60 ℃; for 192h;
DOI:10.1021/jm030873e

Reference yield:

: 549505-79-5
octanoic acid (2-methyl-2-nitro-propyl)-amide

: 622374-91-8
N-[4-(octa-O-acetyllactobionamidomethylene)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: SmI₂; methanol / tetrahydrofuran

2: 63 percent / molecular sieves 4 Ae / tetrahydrofuran / 192 h / 60 °C

With methanol; samarium diiodide; 4 A molecular sieve; In tetrahydrofuran;
DOI:10.1021/jm030873e

Reference yield:

: 111-64-8
n-octanoic acid chloride

: 622374-91-8
N-[4-(octa-O-acetyllactobionamidomethylene)benzylidene]-N-[1,1-dimethyl-2-(N-octanoyl)amido]ethylamine N-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / TEA / dimethylformamide / -15 °C

2: SmI₂; methanol / tetrahydrofuran

3: 63 percent / molecular sieves 4 Ae / tetrahydrofuran / 192 h / 60 °C

With methanol; samarium diiodide; 4 A molecular sieve; TEA; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm030873e