N-(1-Acetoxymethylallyl)-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid

Base Information

Chemical Name:N-(1-Acetoxymethylallyl)-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid
CAS No.:74608-07-4
Molecular Formula:C₂₀H₂₄N₂O₆S₃
Molecular Weight:484.618
Hs Code.:

Synonyms:N-(1-Acetoxymethylallyl)-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-Acetoxymethylallyl)-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid

Chemical Property:

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Technology Process of N-(1-Acetoxymethylallyl)-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid

There total 2 articles about N-(1-Acetoxymethylallyl)-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1576-84-7
1-acetoxy-3-butene

: 851-06-9
bis(p-toluenesulfonyl) sulfur diimide

: 74608-07-4
N-(1-Acetoxymethylallyl)-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid

Guidance literature:: In toluene; at 20 ℃; for 10h;

Reference yield:

: 70-55-3
toluene-4-sulfonamide

: 74608-07-4
N-(1-Acetoxymethylallyl)-N-(p-toluolsulfonamidothio)-p-toluolsulfonamid

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / SOCl₂ / various solvent(s) / 1) 8 h, 80 deg C

2: 87 percent / toluene / 10 h / 20 °C

With thionyl chloride; In toluene;