N-{3-[(1-Benzyl-1H-tetrazole-5-carbonyl)-amino]-5-cyano-phenyl}-oxalamic acid ethyl ester

Base Information

Chemical Name:N-{3-[(1-Benzyl-1H-tetrazole-5-carbonyl)-amino]-5-cyano-phenyl}-oxalamic acid ethyl ester
CAS No.:77245-56-8
Molecular Formula:C₂₀H₁₇N₇O₄
Molecular Weight:419.399
Hs Code.:

Synonyms:N-{3-[(1-Benzyl-1H-tetrazole-5-carbonyl)-amino]-5-cyano-phenyl}-oxalamic acid ethyl ester

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Chemical Property of N-{3-[(1-Benzyl-1H-tetrazole-5-carbonyl)-amino]-5-cyano-phenyl}-oxalamic acid ethyl ester

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Technology Process of N-{3-[(1-Benzyl-1H-tetrazole-5-carbonyl)-amino]-5-cyano-phenyl}-oxalamic acid ethyl ester

There total 5 articles about N-{3-[(1-Benzyl-1H-tetrazole-5-carbonyl)-amino]-5-cyano-phenyl}-oxalamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63005-71-0
1-benzyl-1H-tetrazole-5-carboxylic acid ethyl ester

: 77245-56-8
N-{3-[(1-Benzyl-1H-tetrazole-5-carbonyl)-amino]-5-cyano-phenyl}-oxalamic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / KOH / ethanol

2: oxalyl chloride, pyridine / benzene / 0.5 h / 15 °C

3: pyridine / CH₂Cl₂ / 2 h / Ambient temperature

With pyridine; potassium hydroxide; oxalyl dichloride; In ethanol; dichloromethane; benzene;
DOI:10.1021/jm00138a021

Reference yield:

: 63005-72-1
1-benzyl-1H-tetrazole-5-carboxylic acid potassium salt

: 77245-56-8
N-{3-[(1-Benzyl-1H-tetrazole-5-carbonyl)-amino]-5-cyano-phenyl}-oxalamic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride, pyridine / benzene / 0.5 h / 15 °C

2: pyridine / CH₂Cl₂ / 2 h / Ambient temperature

With pyridine; oxalyl dichloride; In dichloromethane; benzene;
DOI:10.1021/jm00138a021

Reference yield:

: 7142-72-5
N-benzyloxamic acid ethyl ester

: 77245-56-8
N-{3-[(1-Benzyl-1H-tetrazole-5-carbonyl)-amino]-5-cyano-phenyl}-oxalamic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: PCl₅, pyridine / CH₂Cl₂ / 1 h / Ambient temperature

2: hydrazoic acid / CH₂Cl₂; benzene / 1.) RT, 1 h, 2.) reflux, 5 h

3: 90 percent / KOH / ethanol

4: oxalyl chloride, pyridine / benzene / 0.5 h / 15 °C

5: pyridine / CH₂Cl₂ / 2 h / Ambient temperature

With pyridine; potassium hydroxide; hydrogen azide; oxalyl dichloride; phosphorus pentachloride; In ethanol; dichloromethane; benzene;
DOI:10.1021/jm00138a021