Tetraethyl 1,2-phenylene bis(phosphate)

Base Information

Chemical Name:Tetraethyl 1,2-phenylene bis(phosphate)
CAS No.:37521-98-5
Molecular Formula:C₁₄H₂₄O₈P₂
Molecular Weight:382.287
Hs Code.:

Synonyms:Tetraethyl 1,2-phenylene bis(phosphate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Tetraethyl 1,2-phenylene bis(phosphate)

Chemical Property:

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Technology Process of Tetraethyl 1,2-phenylene bis(phosphate)

There total 2 articles about Tetraethyl 1,2-phenylene bis(phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.5%

Diethyl phosphonate: 762-04-9,123-22-8
Diethyl phosphonate

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 37521-98-5
Tetraethyl 1,2-phenylene bis(phosphate)

Guidance literature:: With triethylamine; In tetrachloromethane; 1) 0 deg C 2) room temperature;
DOI:10.1021/jo00195a029

Reference yield: 86.6%

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 814-49-3
diethyl chlorophosphate

: 37521-98-5
Tetraethyl 1,2-phenylene bis(phosphate)

Guidance literature:: With triethylamine; In tetrahydrofuran; for 15h;
DOI:10.1002/anie.201310867

Reference yield: 66.5%

: 37521-98-5
Tetraethyl 1,2-phenylene bis(phosphate)

: 91633-17-9
Tetraethyl (2,3-dihydroxy-1,4-phenylene)bis(phosphonate)

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 3h; Cooling with acetone-dry ice;
DOI:10.1002/anie.201310867