[(2-trimethylstannyl)phenyl] diethylphosphate

Base Information

Chemical Name:[(2-trimethylstannyl)phenyl] diethylphosphate
CAS No.:482288-71-1
Molecular Formula:C₁₃H₂₃O₄PSn
Molecular Weight:393.007
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [(2-trimethylstannyl)phenyl] diethylphosphate

Chemical Property:

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Technology Process of [(2-trimethylstannyl)phenyl] diethylphosphate

There total 4 articles about [(2-trimethylstannyl)phenyl] diethylphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16462-86-5
2-(chlorophenyl) diethylphosphate

: 16643-09-7
trimethylstannyl sodium

: 482288-71-1
[(2-trimethylstannyl)phenyl] diethylphosphate

Guidance literature:: With sodium; In ammonia; dissolving of Sn compd. in dried ammonia, addn. of Na metal, addn. of organic phosphate, stirring in the dark for 1.5 h, addn. of aq. ammonium chloride;
DOI:10.1021/om020622o

Reference yield:

: 37521-98-5
Tetraethyl 1,2-phenylene bis(phosphate)

: 16643-09-7
trimethylstannyl sodium

: 482288-71-1
[(2-trimethylstannyl)phenyl] diethylphosphate

Guidance literature:: With sodium; In ammonia; dissolving of Sn compd. in dried ammonia, addn. of Na metal, addn. of organic phosphate, stirring in the dark for 1.5 h, addn. of aq. ammonium chloride;
DOI:10.1021/om020622o

Reference yield:

: 16462-86-5
2-(chlorophenyl) diethylphosphate

: 16643-09-7
trimethylstannyl sodium

: 482288-71-1
[(2-trimethylstannyl)phenyl] diethylphosphate

: 14275-62-8
1,2-bis(trimethylstannyl)benzene

Guidance literature:: With sodium; In ammonia; Irradiation (UV/VIS); dissolving of Sn compd. in dried ammonia, addn. of Na metal, addn. of organic phosphate, irradn. with UV light (350 nm max.) with stirring for up to 1.5 h, addn. of aq. ammonium chloride; evapn. of ammonia, extn. with ether, drying over MgSO4, chromy. (silica gel, hexane/ethyl acetate 50/50); products ratio depends on the time of irradn.;
DOI:10.1021/om020622o