trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methanesulfonyl-pyrimidin-4-yl ester

Base Information

Chemical Name:trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methanesulfonyl-pyrimidin-4-yl ester
CAS No.:871794-86-4
Molecular Formula:C₁₇H₁₇F₃N₂O₅S
Molecular Weight:418.394
Hs Code.:

Synonyms:trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methanesulfonyl-pyrimidin-4-yl ester

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Chemical Property of trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methanesulfonyl-pyrimidin-4-yl ester

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Technology Process of trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methanesulfonyl-pyrimidin-4-yl ester

There total 6 articles about trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methanesulfonyl-pyrimidin-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 871794-85-3
trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methylsulfanyl-pyrimidin-4-yl ester

: 871794-86-4
trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methanesulfonyl-pyrimidin-4-yl ester

Guidance literature:: With potassium peroxymonosulfate; In methanol; water; at 20 ℃;

Reference yield:

: 10385-30-5
4-(benzyloxy)butanoic acid

: 871794-86-4
trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methanesulfonyl-pyrimidin-4-yl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: dmap; cycl-isopropylidene malonate / dichloromethane / 2 h / 0 °C

2.1: Heating / reflux

3.1: sodium methylate / methanol / 0 °C

3.2: Heating / reflux

4.1: potassium hydroxide / methanol / 20 °C

5.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C

6.1: potassium peroxymonosulfate / methanol; water / 20 °C

With dmap; potassium hydroxide; potassium peroxymonosulfate; cycl-isopropylidene malonate; sodium methylate; triethylamine; In methanol; dichloromethane; water;

Reference yield:

: 10378-08-2
ethyl 6-(benzyloxy)-3-oxohexanoate

: 871794-86-4
trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methanesulfonyl-pyrimidin-4-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium methylate / methanol / 0 °C

1.2: Heating / reflux

2.1: potassium hydroxide / methanol / 20 °C

3.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C

4.1: potassium peroxymonosulfate / methanol; water / 20 °C

With potassium hydroxide; potassium peroxymonosulfate; sodium methylate; triethylamine; In methanol; dichloromethane; water;