trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methylsulfanyl-pyrimidin-4-yl ester

Base Information

Chemical Name:trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methylsulfanyl-pyrimidin-4-yl ester
CAS No.:871794-85-3
Molecular Formula:C₁₇H₁₇F₃N₂O₃S
Molecular Weight:386.395
Hs Code.:

Synonyms:trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methylsulfanyl-pyrimidin-4-yl ester

Suppliers and Price of trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methylsulfanyl-pyrimidin-4-yl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methylsulfanyl-pyrimidin-4-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methylsulfanyl-pyrimidin-4-yl ester

There total 5 articles about trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methylsulfanyl-pyrimidin-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 871794-84-2
6-(3-benzyloxy-propyl)-2-methylsulfanyl-pyrimidin-4-ol

: 407-25-0
trifluoroacetic anhydride

: 871794-85-3
trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methylsulfanyl-pyrimidin-4-yl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

: 10385-30-5
4-(benzyloxy)butanoic acid

: 871794-85-3
trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methylsulfanyl-pyrimidin-4-yl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: dmap; cycl-isopropylidene malonate / dichloromethane / 2 h / 0 °C

2.1: Heating / reflux

3.1: sodium methylate / methanol / 0 °C

3.2: Heating / reflux

4.1: potassium hydroxide / methanol / 20 °C

5.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C

With dmap; potassium hydroxide; cycl-isopropylidene malonate; sodium methylate; triethylamine; In methanol; dichloromethane;

Reference yield:

: 10378-08-2
ethyl 6-(benzyloxy)-3-oxohexanoate

: 871794-85-3
trifluoro-acetic acid 6-(3-benzyloxy-propyl)-2-methylsulfanyl-pyrimidin-4-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate / methanol / 0 °C

1.2: Heating / reflux

2.1: potassium hydroxide / methanol / 20 °C

3.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C

With potassium hydroxide; sodium methylate; triethylamine; In methanol; dichloromethane;