ethyl (S)-1-4-methyl 2-((2S,5S)-1-benzyl-5-(tert-butoxycarbonyl)-pyrrolidin-2-yl)succinate

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Chemical Name:ethyl (S)-1-4-methyl 2-((2S,5S)-1-benzyl-5-(tert-butoxycarbonyl)-pyrrolidin-2-yl)succinate
CAS No.:1235568-26-9
Molecular Formula:C₂₃H₃₃NO₆
Molecular Weight:419.518
Hs Code.:

Synonyms:ethyl (S)-1-4-methyl 2-((2S,5S)-1-benzyl-5-(tert-butoxycarbonyl)-pyrrolidin-2-yl)succinate

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Chemical Property of ethyl (S)-1-4-methyl 2-((2S,5S)-1-benzyl-5-(tert-butoxycarbonyl)-pyrrolidin-2-yl)succinate

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Technology Process of ethyl (S)-1-4-methyl 2-((2S,5S)-1-benzyl-5-(tert-butoxycarbonyl)-pyrrolidin-2-yl)succinate

There total 1 articles about ethyl (S)-1-4-methyl 2-((2S,5S)-1-benzyl-5-(tert-butoxycarbonyl)-pyrrolidin-2-yl)succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1235568-24-7
tert-butyl (2S,5S)-1-benzyl-5-(2-ethoxycarbonylmethyl)pyrrolidine-2-carboxylate

: 96-32-2
bromoacetic acid methyl ester

: 1235568-26-9
ethyl (S)-1-4-methyl 2-((2S,5S)-1-benzyl-5-(tert-butoxycarbonyl)-pyrrolidin-2-yl)succinate

Guidance literature:: tert-butyl (2S,5S)-1-benzyl-5-(2-ethoxycarbonylmethyl)pyrrolidine-2-carboxylate; With lithium hexamethyldisilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.75h; Inert atmosphere;

bromoacetic acid methyl ester; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; toluene; at -78 ℃; for 0.666667h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/jo1008433