Acetic acid cyano-(4-methoxy-2,6-dimethyl-phenyl)-methyl ester

Base Information

• Chemical Name: Acetic acid cyano-(4-methoxy-2,6-dimethyl-phenyl)-methyl ester
• CAS No.: 92516-26-2
• Molecular Formula: C₁₃H₁₅NO₃
• Molecular Weight: 233.267
• Mol file: 92516-26-2.mol

Synonyms:Acetic acid cyano-(4-methoxy-2,6-dimethyl-phenyl)-methyl ester

Chemical Property of Acetic acid cyano-(4-methoxy-2,6-dimethyl-phenyl)-methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Acetic acid cyano-(4-methoxy-2,6-dimethyl-phenyl)-methyl ester

There total 2 articles about Acetic acid cyano-(4-methoxy-2,6-dimethyl-phenyl)-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

Cyanhydrin von 2.6-Dimethyl-4-methoxybenzaldehyd (70242-29-4) + acetic anhydride (108-24-7) → Acetic acid cyano-(4-methoxy-2,6-dimethyl-phenyl)-methyl ester (92516-26-2)

Guidance literature:

In pyridine;

DOI:10.1246/bcsj.57.1510

Reference yield:

4-methoxy-2,6-dimethylbenzylaldehyde (19447-00-8) → Acetic acid cyano-(4-methoxy-2,6-dimethyl-phenyl)-methyl ester (92516-26-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / CaO / 2 h / 50 °C

2: 98 percent / pyridine

With calcium oxide; In pyridine;

DOI:10.1246/bcsj.57.1510

Reference yield: 93.0%

Acetic acid cyano-(4-methoxy-2,6-dimethyl-phenyl)-methyl ester (92516-26-2) → 1,3-dibromo-6-methoxy-2,4-dimethylbenzene (83385-81-3) + Acetic acid (3-bromo-4-methoxy-2,6-dimethyl-phenyl)-cyano-methyl ester

Guidance literature:

With bromine; potassium bromide; In water; acetic acid; at 60 ℃; for 1h; Product distribution; other temperature;

DOI:10.1246/bcsj.57.1510

upstream raw materials:

Cyanhydrin von 2.6-Dimethyl-4-methoxybenzaldehyd

acetic anhydride

4-methoxy-2,6-dimethylbenzylaldehyde

Downstream raw materials:

2,4,6-tribromo-3,5-dimethylphenol

1,3-dibromo-6-methoxy-2,4-dimethylbenzene

2,4,6-tribromo-3,5-dimethylmethoxybenzene