N-(2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinoline-1-yl)-2-chloroacetamide

Base Information

• Chemical Name: N-(2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinoline-1-yl)-2-chloroacetamide
• CAS No.: 1338471-65-0
• Molecular Formula: C₂₄H₂₄ClN₃O₃S
• Molecular Weight: 469.992

Synonyms:N-(2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinoline-1-yl)-2-chloroacetamide

Chemical Property of N-(2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinoline-1-yl)-2-chloroacetamide

Chemical Property:

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Technology Process of N-(2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinoline-1-yl)-2-chloroacetamide

There total 1 articles about N-(2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinoline-1-yl)-2-chloroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-amino-2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinoline (55023-30-8) + chloroacetyl chloride (79-04-9) → N-(2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinoline-1-yl)-2-chloroacetamide (1338471-65-0)

Guidance literature:

In 1,4-dioxane; for 2h; Heating;

DOI:10.1002/jccs.201190019

Reference yield: 93.0%

N-(2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinoline-1-yl)-2-chloroacetamide (1338471-65-0) → 5-morpholin-4-yl-8-phenyl-1,2,3,4,10-pentahydro[1,4]-diazepino[5',6':4,5]thieno[2,3-c]isoquinolin-11(12H)-one (1338471-66-1)

Guidance literature:

With hexamethylenetetramine; In ethanol; for 20h; Reflux;

DOI:10.1002/jccs.201190019

Reference yield: 87.0%

morpholine (110-91-8,99108-56-2) + N-(2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinoline-1-yl)-2-chloroacetamide (1338471-65-0) → N-(2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinolin-1-yl)-2-morpholin-4-yl-acetamide (1338471-70-7)

Guidance literature:

In ethanol; for 2h; Reflux;

DOI:10.1002/jccs.201190019

upstream raw materials:

1-amino-2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinoline

chloroacetyl chloride

Downstream raw materials:

N-(2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinolin-1-yl)-2-piperidin-4-yl-acetamide

N-(2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinolin-1-yl)-2-morpholin-4-yl-acetamide

5-morpholin-4-yl-8-phenyl-1,2,3,4,10-pentahydro[1,4]-diazepino[5',6':4,5]thieno[2,3-c]isoquinolin-11(12H)-one

N-(2-benzoyl-5-morpholin-4-yl-6,7,8,9-tetrahydrothieno[2,3-c]isoquinolin-1-yl)-2-diethylaminoacetamide

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