3-[(4-chlorophenyl)sulfinyl]-1-methyl-2-[(prop-2-enyl)sulfanyl]-1H-indole

Base Information

Chemical Name:3-[(4-chlorophenyl)sulfinyl]-1-methyl-2-[(prop-2-enyl)sulfanyl]-1H-indole
CAS No.:1449023-31-7
Molecular Formula:C₁₈H₁₆ClNOS₂
Molecular Weight:361.916
Hs Code.:

Synonyms:3-[(4-chlorophenyl)sulfinyl]-1-methyl-2-[(prop-2-enyl)sulfanyl]-1H-indole

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Chemical Property of 3-[(4-chlorophenyl)sulfinyl]-1-methyl-2-[(prop-2-enyl)sulfanyl]-1H-indole

Chemical Property:

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Technology Process of 3-[(4-chlorophenyl)sulfinyl]-1-methyl-2-[(prop-2-enyl)sulfanyl]-1H-indole

There total 7 articles about 3-[(4-chlorophenyl)sulfinyl]-1-methyl-2-[(prop-2-enyl)sulfanyl]-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₁₄ClNOS₂

: 74-88-4
methyl iodide

: 1449023-31-7
3-[(4-chlorophenyl)sulfinyl]-1-methyl-2-[(prop-2-enyl)sulfanyl]-1H-indole

Guidance literature:: In tetrahydrofuran; dimethyl sulfoxide; mineral oil; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.tet.2013.07.011

Reference yield:

: 104292-18-4
N-[2-(chloromethyl)phenyl]formamide

: 1449023-31-7
3-[(4-chlorophenyl)sulfinyl]-1-methyl-2-[(prop-2-enyl)sulfanyl]-1H-indole

Guidance literature:: Multi-step reaction with 6 steps

1.1: N,N-dimethyl-formamide / 0 °C

2.1: sodium periodate / water; methanol / 20 °C

3.1: trichlorophosphate; triethylamine / tetrahydrofuran / 0 °C

4.1: sulfur; selenium; triethylamine / tetrahydrofuran / 20 °C

5.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 0.08 h / 0 °C

5.2: 1 h / 0 - 20 °C

6.1: tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 - 20 °C

With sulfur; selenium; sodium periodate; sodium hydride; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tet.2013.07.011

Reference yield:

: 18803-44-6
sodium p-chlorothiophenolate

: 1449023-31-7
3-[(4-chlorophenyl)sulfinyl]-1-methyl-2-[(prop-2-enyl)sulfanyl]-1H-indole

Guidance literature:: Multi-step reaction with 6 steps

1.1: N,N-dimethyl-formamide / 0 °C

2.1: sodium periodate / water; methanol / 20 °C

3.1: trichlorophosphate; triethylamine / tetrahydrofuran / 0 °C

4.1: sulfur; selenium; triethylamine / tetrahydrofuran / 20 °C

5.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 0.08 h / 0 °C

5.2: 1 h / 0 - 20 °C

6.1: tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 - 20 °C

With sulfur; selenium; sodium periodate; sodium hydride; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tet.2013.07.011