acetic acid cyclopent-3-enylmethyl ester

Base Information

• Chemical Name: acetic acid cyclopent-3-enylmethyl ester
• CAS No.: 298227-78-8
• Molecular Formula: C₈H₁₂O₂
• Molecular Weight: 140.182
• Mol file: 298227-78-8.mol

Synonyms:acetic acid cyclopent-3-enylmethyl ester

Chemical Property of acetic acid cyclopent-3-enylmethyl ester

Chemical Property:

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Technology Process of acetic acid cyclopent-3-enylmethyl ester

There total 1 articles about acetic acid cyclopent-3-enylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

4-(hydroxymethyl)cyclopentene (25125-21-7) + acetic anhydride (108-24-7) → acetic acid cyclopent-3-enylmethyl ester (298227-78-8)

Guidance literature:

With pyridine; at 18 ℃; for 16h;

DOI:10.1039/b002525i

Reference yield:

4-methoxybenzenediazonium tetrafluoroborate (459-64-3) + acetic acid cyclopent-3-enylmethyl ester (298227-78-8) → C13H16O2 + ((1S,4R)-4-(4-methoxyphenyl)cyclopent-2-en-1-yl)methanol

Guidance literature:

4-methoxybenzenediazonium tetrafluoroborate; acetic acid cyclopent-3-enylmethyl ester; With 2,6-di-tert-butyl-4-methylpyridine; pyrabox; Pd*2C₂HF₃O₂; zinc(II) carbonate; In methanol; toluene; at 60 ℃; for 48h;

With sodium hydroxide; In methanol; ethanol; toluene; at 20 ℃; for 0.5h; Overall yield = 27 %;

DOI:10.1002/chem.201801910

Reference yield:

1-(4-acetylphenyl)diazonium tetrafluoroborate (350-47-0) + acetic acid cyclopent-3-enylmethyl ester (298227-78-8) → C14H16O2 + (4-((1R,4S)-4-(hydroxymethyl)cyclopent-2-en-1-yl)phenyl)ethan-1-one

Guidance literature:

1-(4-acetylphenyl)diazonium tetrafluoroborate; acetic acid cyclopent-3-enylmethyl ester; With 2,6-di-tert-butyl-4-methylpyridine; pyrabox; Pd*2C₂HF₃O₂; zinc(II) carbonate; In methanol; toluene; at 60 ℃; for 48h;

With sodium hydroxide; In methanol; ethanol; toluene; at 20 ℃; for 0.5h; Overall yield = 12 %;

DOI:10.1002/chem.201801910

upstream raw materials:

4-(hydroxymethyl)cyclopentene

acetic anhydride