pyroglutamyl-alanyl-N^ε-benzyloxycarbonyllysyl-serine hydrazide

Base Information

Chemical Name:pyroglutamyl-alanyl-N^ε-benzyloxycarbonyllysyl-serine hydrazide
CAS No.:111705-67-0
Molecular Formula:C₂₅H₃₇N₇O₈
Molecular Weight:563.611
Hs Code.:

pyroglutamyl-alanyl-N<sup>ε</sup>-benzyloxycarbonyllysyl-serine hydrazide

Synonyms:pyroglutamyl-alanyl-N^ε-benzyloxycarbonyllysyl-serine hydrazide

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Chemical Property of pyroglutamyl-alanyl-N^ε-benzyloxycarbonyllysyl-serine hydrazide

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Technology Process of pyroglutamyl-alanyl-N^ε-benzyloxycarbonyllysyl-serine hydrazide

There total 3 articles about pyroglutamyl-alanyl-N^ε-benzyloxycarbonyllysyl-serine hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 111705-66-9
pyroglutamyl-alanyl-N^ε-benzyloxycarbonyllysyl-serine methyl ester

: 111705-67-0
pyroglutamyl-alanyl-N^ε-benzyloxycarbonyllysyl-serine hydrazide

Guidance literature:: With hydrazine hydrate; In methanol; N,N-dimethyl-formamide; for 8h; Ambient temperature;

Reference yield:

: 111705-65-8
alanyl-N^ε-benzyloxycarbonyllysyl-serine methyl ester hydrochloride

: 111705-67-0
pyroglutamyl-alanyl-N^ε-benzyloxycarbonyllysyl-serine hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 1-hydroxybenztriazole, N,N'-dicyclohexylcarbodiimide; 2) N-ethylpiperidine / 1) DMF, 10 min., -10 deg C; 2) 2 h, 0 deg C, then 8 h, room temp.

2: 79 percent / hydrazine hydrate / dimethylformamide; methanol / 8 h / Ambient temperature

With 1-ethyl-piperidine; benzotriazol-1-ol; hydrazine hydrate; dicyclohexyl-carbodiimide; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 84983-67-5
tert.-butyloxycarbonylalanyl-N^ε-benzyloxycarbonyllysyl-serine methyl ester

: 111705-67-0
pyroglutamyl-alanyl-N^ε-benzyloxycarbonyllysyl-serine hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / 1 M HCl in CH₃COOH / acetic acid / 1 h / Ambient temperature

2: 1) 1-hydroxybenztriazole, N,N'-dicyclohexylcarbodiimide; 2) N-ethylpiperidine / 1) DMF, 10 min., -10 deg C; 2) 2 h, 0 deg C, then 8 h, room temp.

3: 79 percent / hydrazine hydrate / dimethylformamide; methanol / 8 h / Ambient temperature

With 1-ethyl-piperidine; hydrogenchloride; benzotriazol-1-ol; hydrazine hydrate; dicyclohexyl-carbodiimide; In methanol; acetic acid; N,N-dimethyl-formamide;