Technology Process of C25H26Cl2N6O
There total 6 articles about C25H26Cl2N6O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 50 ℃;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trichlorophosphate / 1,4-dioxane / 3 h / 40 - 80 °C
1.2: 0 °C
2.1: hydrogen / palladium dihydroxide / methanol / 6 h
3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 50 °C
With
hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trichlorophosphate;
palladium dihydroxide;
In
1,4-dioxane; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride; water / 17 h / 100 °C
2.1: O?(6?chlorobezotriazol?1?yl)?N,N,N,N?tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; 6-chloro-1-hydroxybenzotriazole / N,N-dimethyl-formamide / 17.08 h / 20 °C
3.1: trichlorophosphate / 1,4-dioxane / 3 h / 40 - 80 °C
3.2: 0 °C
4.1: hydrogen / palladium dihydroxide / methanol / 6 h
5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 50 °C
With
hydrogenchloride; O?(6?chlorobezotriazol?1?yl)?N,N,N,N?tetramethyluronium hexafluorophosphate; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 6-chloro-1-hydroxybenzotriazole; trichlorophosphate;
palladium dihydroxide;
In
1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;