C₅H₅Ru(PC₆H₅(CH₃)2)2SiClHCH₃

Base Information

• Chemical Name: C₅H₅Ru(PC₆H₅(CH₃)2)2SiClHCH₃
• CAS No.: 475635-26-8
• Molecular Formula: C₂₂H₃₁ClP₂RuSi
• Molecular Weight: 522.044

Synonyms:C₅H₅Ru(PC₆H₅(CH₃)2)2SiClHCH₃

Chemical Property of C₅H₅Ru(PC₆H₅(CH₃)2)2SiClHCH₃

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Technology Process of C₅H₅Ru(PC₆H₅(CH₃)2)2SiClHCH₃

There total 2 articles about C₅H₅Ru(PC₆H₅(CH₃)2)2SiClHCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Dichloromethylsilane (75-54-7) + Ru(C5H5)H(P(CH3)2C6H5)2 (310896-06-1) → C5H5Ru(PC6H5(CH3)2)2SiClHCH3 (475635-26-8)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; byproducts: 1,8-diazabicyclo[5.4.0]undec-7-enium chloride; (Ar); addn. of silicon compd. to a frozen soln. of ruthenium complex andDBU in CH2Cl2, warming to room temp., stirring for 1.5 h; evapn., extn. with Et2O, filtration through Celite, concn., addn. of hexanes, concn., filtration, drying in vac.; elem. anal.;

DOI:10.1021/om0204235

Reference yield:

Dichloromethylsilane (75-54-7) + Ru(C5H5)H(P(CH3)2C6H5)2 (310896-06-1) → C5H5Ru(PC6H5(CH3)2)2H2(1+)*Cl(1-)=[C5H5Ru(PC6H5(CH3)2)2H2]Cl (475635-34-8) + C5H5Ru(PC6H5(CH3)2)2SiClHCH3 (475635-26-8)

Guidance literature:

In dichloromethane; (Ar); addn. of CH2Cl2 to ruthenium complex, addn. of silicon compd. to afrozen soln., slow warming to room temp., stirring for 15 min; concn., addn. of hexanes, filtration, evapn., obtained as a mixt. of complexes;

DOI:10.1021/om0204235

Reference yield: 80.0%

lithium aluminium tetrahydride (16853-85-3) + C5H5Ru(PC6H5(CH3)2)2SiClHCH3 (475635-26-8) → C5H5Ru(PC6H5(CH3)2)2SiH2CH3 (475635-30-4)

Guidance literature:

In diethyl ether; (Ar); addn. of Et2O to a mixt. of ruthenium complex and LiAlH4, stirringfor 1.5 h at room temp.; evapn., extn. with hexanes, filtration through Celite, evapn., elem. anal.;

DOI:10.1021/om0204235

upstream raw materials:

Dichloromethylsilane

Ru(C₅H₅)H(P(CH₃)2C₆H₅)2

Downstream raw materials:

C₅H₅Ru(PC₆H₅(CH₃)2)2SiH₂CH₃

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