C₄₅H₆₈N₄O₈

Base Information

Chemical Name:C₄₅H₆₈N₄O₈
CAS No.:1613707-35-9
Molecular Formula:C₄₅H₆₈N₄O₈
Molecular Weight:793.057
Hs Code.:

C<sub>45</sub>H<sub>68</sub>N<sub>4</sub>O<sub>8</sub>

Synonyms:C₄₅H₆₈N₄O₈

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Chemical Property of C₄₅H₆₈N₄O₈

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Technology Process of C₄₅H₆₈N₄O₈

There total 17 articles about C₄₅H₆₈N₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1613707-34-8
C₅₃H₇₀N₄O₁₀

: 1613707-35-9
C₄₅H₆₈N₄O₈

Guidance literature:: With palladium 10% on activated carbon; hydrogen; acetic acid; In ethanol; at 20 ℃; for 4h; under 760.051 Torr;

Reference yield:

: (Z)-methyl 2-(tert-butyloxycarbonyl)amino-3-(1-(tert-butyldimethylsilyloxy)naphthalen-4-yl)acrylate

: 1613707-35-9
C₄₅H₆₈N₄O₈

Guidance literature:: Multi-step reaction with 8 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 20 °C / 760.05 Torr

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C

3: CHIRAEPAKAD columnS cm I_.Dx₅₀ cm L / isopropyl alcohol; n-heptane / Resolution of racemate

4: pyridine / 2 h / 0 - 20 °C

5: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

6: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

7: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

8: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol / 4 h / 20 °C / 760.05 Torr

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; water; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; n-heptane; isopropyl alcohol; acetonitrile;

Reference yield:

: 1613707-21-3
methyl 2-(tert-butoxycarbonylamino)-3-(4-(tert-butyldimethylsilyloxy)naphthalen-1-yl)propanoate

: 1613707-35-9
C₄₅H₆₈N₄O₈

Guidance literature:: Multi-step reaction with 7 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C

2: CHIRAEPAKAD columnS cm I_.Dx₅₀ cm L / isopropyl alcohol; n-heptane / Resolution of racemate

3: pyridine / 2 h / 0 - 20 °C

4: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

5: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

6: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

7: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol / 4 h / 20 °C / 760.05 Torr

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; water; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; n-heptane; isopropyl alcohol; acetonitrile;