(1E,5E)-1-(4-methoxybenzyloxy)-6-methoxymethoxy-3,4-dimethylenehexa-1,5-diene

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Chemical Name:(1E,5E)-1-(4-methoxybenzyloxy)-6-methoxymethoxy-3,4-dimethylenehexa-1,5-diene
CAS No.:1361253-98-6
Molecular Formula:C₁₈H₂₂O₄
Molecular Weight:302.37
Hs Code.:

Synonyms:(1E,5E)-1-(4-methoxybenzyloxy)-6-methoxymethoxy-3,4-dimethylenehexa-1,5-diene

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Chemical Property of (1E,5E)-1-(4-methoxybenzyloxy)-6-methoxymethoxy-3,4-dimethylenehexa-1,5-diene

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Technology Process of (1E,5E)-1-(4-methoxybenzyloxy)-6-methoxymethoxy-3,4-dimethylenehexa-1,5-diene

There total 7 articles about (1E,5E)-1-(4-methoxybenzyloxy)-6-methoxymethoxy-3,4-dimethylenehexa-1,5-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1361254-13-8
(4S,5S)-4-(4-methoxybenzyloxy)-5-methoxymethoxy-1,2,6,7-octatetraene

: 1361253-98-6
(1E,5E)-1-(4-methoxybenzyloxy)-6-methoxymethoxy-3,4-dimethylenehexa-1,5-diene

: (3S,4S)-3-(4-methoxybenzyloxy)-4-(methoxymethoxy)bicyclo[4.2.0]octa-1,5-diene

Guidance literature:: With diisopropylamine; copper(ll) bromide; In 1,4-dioxane; at 20 ℃; for 3h; Inert atmosphere; Reflux;
DOI:10.1021/ol300096u

Reference yield: 46.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1361254-23-0
(3S,4S)-3-(4-methoxybenzyloxy)-4-(methoxymethoxy)hexa-1,5-diyne

: 1361253-98-6
(1E,5E)-1-(4-methoxybenzyloxy)-6-methoxymethoxy-3,4-dimethylenehexa-1,5-diene

: (3S,4S)-3-(4-methoxybenzyloxy)-4-(methoxymethoxy)bicyclo[4.2.0]octa-1,5-diene

Guidance literature:: With diisopropylamine; copper(I) bromide; In 1,4-dioxane; for 4.5h; Inert atmosphere; Reflux;
DOI:10.1021/ol300096u

Reference yield:

: 220271-25-0
(4S,5S)-4,5-diethynyl-2-(4-methoxyphenyl)-1,3-dioxolane

: 1361253-98-6
(1E,5E)-1-(4-methoxybenzyloxy)-6-methoxymethoxy-3,4-dimethylenehexa-1,5-diene

: (3S,4S)-3-(4-methoxybenzyloxy)-4-(methoxymethoxy)bicyclo[4.2.0]octa-1,5-diene

Guidance literature:: Multi-step reaction with 4 steps

1: diisopropylamine; copper(I) bromide / 1,4-dioxane / 3 h / 20 °C / Inert atmosphere; Reflux

2: diisobutylaluminium hydride / hexane; toluene / 2 h / -78 °C / Inert atmosphere

3: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

4: diisopropylamine; copper(ll) bromide / 1,4-dioxane / 3 h / 20 °C / Inert atmosphere; Reflux

With tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; diisopropylamine; N-ethyl-N,N-diisopropylamine; copper(I) bromide; copper(ll) bromide; In 1,4-dioxane; hexane; dichloromethane; toluene;
DOI:10.1021/ol300096u