Phenylaminothioxoacetic Acid

Base Information

• Chemical Name: Phenylaminothioxoacetic Acid
• CAS No.: 6890-75-1
• Molecular Formula: C₈H₇NO₂S
• Molecular Weight: 181.215

Synonyms:Phenylaminothioxoacetic Acid

Chemical Property of Phenylaminothioxoacetic Acid

Chemical Property:

Purity/Quality:

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Technology Process of Phenylaminothioxoacetic Acid

There total 12 articles about Phenylaminothioxoacetic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2,2,2-Tris-benzotriazol-1-yl-N-phenyl-thioacetamide (130749-24-5) → Phenylaminothioxoacetic Acid (6890-75-1)

Guidance literature:

With sulfuric acid; In tetrahydrofuran; at 50 ℃; for 48h;

DOI:10.1055/s-1990-26975

Reference yield:

N-phenyl-mercaptoacetamide disulfide (3095-79-2) + furan-2,3,5(4H)-trione pyridine (1:1) → 2-mercapto-N-phenylacetamide (4822-44-0) + N,N'-diphenylthiooxamide (78121-70-7) + Phenylaminothioxoacetic Acid (6890-75-1)

Guidance literature:

Reference yield:

2-thioxo-2-phenylaminoacetic acid ethyl ester (56934-77-1) → Phenylaminothioxoacetic Acid (6890-75-1)

Guidance literature:

With water; sodium hydroxide; In dichloromethane; at 0 - 25 ℃; for 2h;

DOI:10.1016/j.bmc.2015.08.019

upstream raw materials:

Ethyl oxanilate

N-Phenyldithiooxamide

2-(phenylamino)-2-thiooxoacetamide

N-phenyl-mercaptoacetamide disulfide

Downstream raw materials:

isothiocyanatobenzene

N,N'-diphenylformamidine

oxanilic acid

hydrogen sulfide

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