2,2'-anhydro-3-(3,5-di-O-mesyl-β-D-arabinofuranosyl)-6,7-diphenyllumazine

Base Information

Chemical Name:2,2'-anhydro-3-(3,5-di-O-mesyl-β-D-arabinofuranosyl)-6,7-diphenyllumazine
CAS No.:92955-40-3
Molecular Formula:C₂₅H₂₂N₄O₉S₂
Molecular Weight:586.603
Hs Code.:

Synonyms:2,2'-anhydro-3-(3,5-di-O-mesyl-β-D-arabinofuranosyl)-6,7-diphenyllumazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2'-anhydro-3-(3,5-di-O-mesyl-β-D-arabinofuranosyl)-6,7-diphenyllumazine

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Technology Process of 2,2'-anhydro-3-(3,5-di-O-mesyl-β-D-arabinofuranosyl)-6,7-diphenyllumazine

There total 12 articles about 2,2'-anhydro-3-(3,5-di-O-mesyl-β-D-arabinofuranosyl)-6,7-diphenyllumazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 92982-84-8
6,7-diphenyl-3-(2,3,5-tri-O-mesyl-β-D-ribofuranosyl)lumazine

: 92955-41-4
2,2'-anhydro-3-(5-O-mesyl-β-D-arabinofuranosyl)-6,7-diphenyllumazine

: 92955-40-3
2,2'-anhydro-3-(3,5-di-O-mesyl-β-D-arabinofuranosyl)-6,7-diphenyllumazine

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 0.166667h; Heating;
DOI:10.1016/0008-6215(84)85279-9

Reference yield: 71.0%

: 124-63-0
methanesulfonyl chloride

: 92955-36-7
2,2'-anhydro-3-β-D-arabinofuranosyl-6,7-dimethyllumazine

: 92955-40-3
2,2'-anhydro-3-(3,5-di-O-mesyl-β-D-arabinofuranosyl)-6,7-diphenyllumazine

Guidance literature:: With pyridine; for 1.5h; Ambient temperature;
DOI:10.1016/0008-6215(84)85279-9

Reference yield:

: 35777-52-7
6,7-diphenyl-1,3-bis(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)lumazine

: 92955-40-3
2,2'-anhydro-3-(3,5-di-O-mesyl-β-D-arabinofuranosyl)-6,7-diphenyllumazine

Guidance literature:: Multi-step reaction with 4 steps

1: 17 percent / boron trifluoride etherate / benzene / 12 h

2: 88 percent / sodium, methanol / 16 h / Ambient temperature

3: 87 percent / pyridine / 2 h / Ambient temperature

4: 73 percent / NaHCO₃ / dimethylformamide / 0.17 h / Heating

With pyridine; methanol; sodium; sodium hydrogencarbonate; boron trifluoride diethyl etherate; In N,N-dimethyl-formamide; benzene;
DOI:10.1016/0008-6215(84)85279-9