1-diphenylmethylen-4-[4-(3-oxo-4-morpholinyl)phenyl]-2-propylsemicarbazide

Base Information

Chemical Name:1-diphenylmethylen-4-[4-(3-oxo-4-morpholinyl)phenyl]-2-propylsemicarbazide
CAS No.:635301-88-1
Molecular Formula:C₂₇H₂₈N₄O₃
Molecular Weight:456.544
Hs Code.:

Synonyms:1-diphenylmethylen-4-[4-(3-oxo-4-morpholinyl)phenyl]-2-propylsemicarbazide

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Chemical Property of 1-diphenylmethylen-4-[4-(3-oxo-4-morpholinyl)phenyl]-2-propylsemicarbazide

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Technology Process of 1-diphenylmethylen-4-[4-(3-oxo-4-morpholinyl)phenyl]-2-propylsemicarbazide

There total 3 articles about 1-diphenylmethylen-4-[4-(3-oxo-4-morpholinyl)phenyl]-2-propylsemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 107-08-4
1-iodo-propane

: 635301-87-0
1-diphenylmethylen-4-[4-(3-oxo-4-morpholinyl)phenyl]semicarbazide

: 635301-88-1
1-diphenylmethylen-4-[4-(3-oxo-4-morpholinyl)phenyl]-2-propylsemicarbazide

Guidance literature:: 1-diphenylmethylen-4-[4-(3-oxo-4-morpholinyl)phenyl]semicarbazide; With caesium carbonate; In acetonitrile; at 20 ℃; for 0.5h;

1-iodo-propane; In acetonitrile; for 7h;
DOI:10.1016/j.bmcl.2003.08.007

Reference yield:

: 5350-57-2
benzophenone hydrazone

: 635301-88-1
1-diphenylmethylen-4-[4-(3-oxo-4-morpholinyl)phenyl]-2-propylsemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3.94 g / ethyldiisopropylamine / CH₂Cl₂ / 2 h / 20 °C

2.1: Cs₂CO₃ / acetonitrile / 0.5 h / 20 °C

2.2: 97 percent / acetonitrile / 7 h

With caesium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2003.08.007

Reference yield:

: 635301-86-9
[4-(3-oxo-morpholin-4-yl)-phenyl]-carbamic acid 4-nitro-phenyl ester

: 635301-88-1
1-diphenylmethylen-4-[4-(3-oxo-4-morpholinyl)phenyl]-2-propylsemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3.94 g / ethyldiisopropylamine / CH₂Cl₂ / 2 h / 20 °C

2.1: Cs₂CO₃ / acetonitrile / 0.5 h / 20 °C

2.2: 97 percent / acetonitrile / 7 h

With caesium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2003.08.007